C₆₂H₇₆O₁₁Si

Base Information

Chemical Name:C₆₂H₇₆O₁₁Si
CAS No.:1350309-63-5
Molecular Formula:C₆₂H₇₆O₁₁Si
Molecular Weight:1025.36
Hs Code.:

C<sub>62</sub>H<sub>76</sub>O<sub>11</sub>Si

Synonyms:

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Chemical Property of C₆₂H₇₆O₁₁Si

Chemical Property:

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Technology Process of C₆₂H₇₆O₁₁Si

There total 23 articles about C₆₂H₇₆O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350309-62-4
C₄₁H₅₈O₁₁Si

: 100-39-0
benzyl bromide

: 1350309-63-5
C₆₂H₇₆O₁₁Si

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1021/ja208528c

Reference yield:

: 87-72-9,608-45-7,608-46-8,608-47-9,2460-44-8,6748-95-4,6763-34-4,7261-26-9,7283-06-9,7283-07-0,7296-55-1,7296-56-2,7296-58-4,7296-59-5,7296-60-8,7296-61-9,7296-62-0,7322-30-7,10257-31-5,10257-32-6,10257-33-7,10257-34-8,10257-35-9,19982-83-3,20242-88-0,28697-53-2,36562-42-2,41546-41-2,89299-64-9,107655-34-5,115794-06-4,115794-07-5,130550-15-1,130606-21-2
D-Xylose

: 1350309-63-5
C₆₂H₇₆O₁₁Si

Guidance literature:: Multi-step reaction with 15 steps

1: pyridine

2: boron trifluoride diethyl etherate; triethylamine / dichloromethane / 24 h / 0 - 20 °C / Molecular sieve 4A

3: trimethylsilyl trifluoromethanesulfonate / chloroform-d1 / 26 h

4: sodium methylate / methanol / 16 h / 20 °C / Inert atmosphere

5: CSA / N,N-dimethyl-formamide / 18 h / 20 °C

6: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 0 - 20 °C / Inert atmosphere

7: pyridinium p-toluenesulfonate / isopropyl alcohol / 72 h / 20 °C / Inert atmosphere

8: pyridine; dmap / 1.5 h / 0 - 20 °C / Inert atmosphere

9: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

10: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 4 h / 0 - 20 °C / Molecular sieve 4A; Inert atmosphere

11: 2,6-di-tert-butyl-4-methylpyridine; methyl trifluoromethanesulfonate / dichloromethane / 20 h / 40 °C / Inert atmosphere; Molecular sieve 4A

12: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C

13: pyridine / 1 h / 20 °C

14: sodium methylate / tetrahydrofuran; methanol / 4 h / 0 - 20 °C

15: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With pyridine; 1H-imidazole; dmap; 2,6-di-tert-butyl-4-methylpyridine; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium methylate; pyridinium p-toluenesulfonate; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; In tetrahydrofuran; methanol; chloroform-d1; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/ja208528c

Reference yield:

: 62446-93-9
1,2,3,4-tetra-O-acetyl-D-xylopyranose

: 1350309-63-5
C₆₂H₇₆O₁₁Si

Guidance literature:: Multi-step reaction with 14 steps

1: boron trifluoride diethyl etherate; triethylamine / dichloromethane / 24 h / 0 - 20 °C / Molecular sieve 4A

2: trimethylsilyl trifluoromethanesulfonate / chloroform-d1 / 26 h

3: sodium methylate / methanol / 16 h / 20 °C / Inert atmosphere

4: CSA / N,N-dimethyl-formamide / 18 h / 20 °C

5: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 0 - 20 °C / Inert atmosphere

6: pyridinium p-toluenesulfonate / isopropyl alcohol / 72 h / 20 °C / Inert atmosphere

7: pyridine; dmap / 1.5 h / 0 - 20 °C / Inert atmosphere

8: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

9: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 4 h / 0 - 20 °C / Molecular sieve 4A; Inert atmosphere

10: 2,6-di-tert-butyl-4-methylpyridine; methyl trifluoromethanesulfonate / dichloromethane / 20 h / 40 °C / Inert atmosphere; Molecular sieve 4A

11: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C

12: pyridine / 1 h / 20 °C

13: sodium methylate / tetrahydrofuran; methanol / 4 h / 0 - 20 °C

14: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With pyridine; 1H-imidazole; dmap; 2,6-di-tert-butyl-4-methylpyridine; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium methylate; pyridinium p-toluenesulfonate; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl trifluoromethanesulfonate; In tetrahydrofuran; methanol; chloroform-d1; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/ja208528c