Technology Process of (10-aminodecanoyl)-Ser-Lys-2-cyclohexylethylamide
There total 4 articles about (10-aminodecanoyl)-Ser-Lys-2-cyclohexylethylamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ammonium hydroxide
2.1: sodium hydroxide / water; tert-butyl alcohol / 48 h / 20 °C
3.1: piperidine / N,N-dimethyl-formamide / 0.17 h
3.2: 20 °C
4.1: water; trifluoroacetic acid; chlorotriisopropylsilane / 1 h
With
piperidine; ammonium hydroxide; chlorotriisopropylsilane; water; trifluoroacetic acid; sodium hydroxide;
In
water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1039/c4ob01669f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide / water; tert-butyl alcohol / 48 h / 20 °C
2.1: piperidine / N,N-dimethyl-formamide / 0.17 h
2.2: 20 °C
3.1: water; trifluoroacetic acid; chlorotriisopropylsilane / 1 h
With
piperidine; chlorotriisopropylsilane; water; trifluoroacetic acid; sodium hydroxide;
In
water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1039/c4ob01669f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 72 h / 20 °C / 760.05 Torr
2.1: piperidine / N,N-dimethyl-formamide / 0.17 h
2.2: 20 °C
3.1: water; trifluoroacetic acid; chlorotriisopropylsilane / 1 h
With
piperidine; chlorotriisopropylsilane; palladium 10% on activated carbon; water; hydrogen; trifluoroacetic acid;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1039/c4ob01669f
