5-Cyan-o-veratrumaldehyd

Base Information

• Chemical Name: 5-Cyan-o-veratrumaldehyd
• CAS No.: 100084-07-9
• Molecular Formula: C₁₀H₉NO₃
• Molecular Weight: 191.186
• Mol file: 100084-07-9.mol

Synonyms:

Chemical Property of 5-Cyan-o-veratrumaldehyd

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-Cyan-o-veratrumaldehyd

There total 5 articles about 5-Cyan-o-veratrumaldehyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromo-3-methoxysalicylaldehyde (5034-74-2) → 5-Cyan-o-veratrumaldehyd (100084-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / K₂CO₃ / dimethylformamide / 1.5 h / Ambient temperature

2: 2.) 10percent FeCl₃, HCl / 1.) DMF, 150 deg C, 14 h, 2.) DMF

With hydrogenchloride; iron(III) chloride; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

3-methoxy-2-hydroxybenzaldehyde (148-53-8) → 5-Cyan-o-veratrumaldehyd (100084-07-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / Br₂, KBr / aq. acetic acid / 0.5 h / 110 °C

2: 94 percent / K₂CO₃ / dimethylformamide / 1.5 h / Ambient temperature

3: 2.) 10percent FeCl₃, HCl / 1.) DMF, 150 deg C, 14 h, 2.) DMF

With hydrogenchloride; bromine; iron(III) chloride; potassium carbonate; potassium bromide; In acetic acid; N,N-dimethyl-formamide;

Reference yield:

5-cyano-2,3-dimethoxy-cinnamic acid → 5-Cyan-o-veratrumaldehyd (100084-07-9)

Guidance literature:

With permanganate(VII) ion; sodium carbonate; benzene;

upstream raw materials:

5-bromo-2,3-dimethoxybenzaldehyde

copper(I) cyanide

5-bromo-3-methoxysalicylaldehyde

3-methoxy-2-hydroxybenzaldehyde

Downstream raw materials:

1,22-Bis<2,3-dimethoxy-5-(10-undecinyl)phenyl>docosan

C₆₆H₁₀₆O₈

1,22-Bis<5-(9-chlornonyl)-2,3-dimethoxyphenyl>docosan

3,3'-(1,22-Docosandiyl)bis(4,5-dimethoxybenzolnonanol)

Refernces