Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid
CAS No.:76909-82-5
Molecular Formula:C₇₈H₈₂N₄O₁₇
Molecular Weight:1347.53
Hs Code.:

Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

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Chemical Property of Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

There total 6 articles about Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 613-90-1
benzoyl cyanide

: 76909-82-5
Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CH₂Cl₂; pyridine / 72 h / 0 °C

2: 1.) Ag₂CO₃, molecular sieves 4 Angstroem, 2.) AgClO₄ / 1.) CH₂Cl₂, r.t., 2.) CH₂Cl₂, 0 deg C; r.t.

With 4 A molecular sieve; silver perchlorate; silver carbonate; In pyridine; dichloromethane;

Reference yield:

: 70209-55-1
benzyl 2-acetamido-3,6-di-O-benzyl-4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

: 76909-82-5
Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / KOH / dimethylformamide / 3 h / 0 °C

2: 89 percent / 90percent CH₃COOH / 2.5 h / 60 °C

3: 92 percent / CH₂Cl₂; pyridine / 72 h / 0 °C

4: 1.) Ag₂CO₃, molecular sieves 4 Angstroem, 2.) AgClO₄ / 1.) CH₂Cl₂, r.t., 2.) CH₂Cl₂, 0 deg C; r.t.

With potassium hydroxide; 4 A molecular sieve; silver perchlorate; acetic acid; silver carbonate; In pyridine; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 76909-82-5
Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / KOH / dimethylformamide / 3 h / 0 °C

2: 89 percent / 90percent CH₃COOH / 2.5 h / 60 °C

3: 92 percent / CH₂Cl₂; pyridine / 72 h / 0 °C

4: 1.) Ag₂CO₃, molecular sieves 4 Angstroem, 2.) AgClO₄ / 1.) CH₂Cl₂, r.t., 2.) CH₂Cl₂, 0 deg C; r.t.

With potassium hydroxide; 4 A molecular sieve; silver perchlorate; acetic acid; silver carbonate; In pyridine; dichloromethane; N,N-dimethyl-formamide;