triphenylantimonybis(2-pyridinecarboxylate)

Base Information

• Chemical Name: triphenylantimonybis(2-pyridinecarboxylate)
• CAS No.: 129763-81-1
• Molecular Formula: C₃₀H₂₃N₂O₄Sb
• Molecular Weight: 597.274
• Mol file: 129763-81-1.mol

Synonyms:

Chemical Property of triphenylantimonybis(2-pyridinecarboxylate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of triphenylantimonybis(2-pyridinecarboxylate)

There total 2 articles about triphenylantimonybis(2-pyridinecarboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-Picolinic acid (98-98-6) + triphenylantimony(V) isopropoxide (785781-58-0) → triphenylantimonybis(2-pyridinecarboxylate) (129763-81-1)

Guidance literature:

In benzene; byproducts: (CH3)2CHOH; (N2); ligand added to a soln. of Sb compd., stirred at room temp.; evapd. (vac.), recrystd. (C6H6/hexane);

DOI:10.1016/j.jorganchem.2007.07.033

Reference yield: 56.0%

2-Picolinic acid (98-98-6) + triphenyl antimony oxide (4756-75-6) → triphenylantimonybis(2-pyridinecarboxylate) (129763-81-1)

Guidance literature:

In chloroform; addn. of 2-pyridinecarboxylic acid in CHCl3 to a suspn. of Ph3SbO in CHCl3, stirring (room temp., 1 h), concg. of soln. (rotary evapn.), addn. of petroleum ether to turbidity, standing in an ice-box (overnight), crystn.; filtration, washing (petroleum ether), drying (vac.); elem. anal.; Kinetics;

upstream raw materials:

2-Picolinic acid

triphenyl antimony oxide

triphenylantimony(V) isopropoxide