(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2*B(C₆H₃(CF₃)2)4

Base Information

• Chemical Name: (C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2*B(C₆H₃(CF₃)2)4
• CAS No.: 314733-85-2
• Molecular Formula: C₂₉H₃₅ClN₃Ru*C₃₂H₁₂BF₂₄
• Molecular Weight: 1425.36

Synonyms:

Chemical Property of (C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2*B(C₆H₃(CF₃)2)4

Chemical Property:

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Technology Process of (C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2*B(C₆H₃(CF₃)2)4

There total 1 articles about (C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCl(C₂H₄)2*B(C₆H₃(CF₃)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

ethene (74-85-1) + [2,6-(2,6-Me2C6H3NCMe)2pyridyl]RuCl2(ethylene) (314733-83-0) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → (C6H3(CH3)2NCCH3)2C5H3NRuCl(C2H4)2(1+)*B(C6H3(CF3)2)4(1-)=(C6H3(CH3)2NCCH3)2C5H3NRuCl(C2H4)2*B(C6H3(CF3)2)4 (314733-85-2)

Guidance literature:

In dichloromethane; byproducts: NaCl; the mixt. in Ch2Cl2 was stirred at room temp. for 2.5 h under C2H4 atm.; filtered, NaCl was washed with CH2Cl2, the combuned fractions were dried in vac., the solid was dissolved in CH2Cl2 under Ar, pentane was added, the mixt. was stirred, cooled to 0°C, filtered; elem. anal.;

DOI:10.1021/om000674i

Reference yield: 73.0%

(C6H3(CH3)2NCCH3)2C5H3NRuCl(C2H4)2(1+)*B(C6H3(CF3)2)4(1-)=(C6H3(CH3)2NCCH3)2C5H3NRuCl(C2H4)2*B(C6H3(CF3)2)4 (314733-85-2) + dimethyl(N,N,N',N'-tetramethylethylenediamine)magnesium + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → (C6H3(CH3)2NCCH3)2C5H3NRuCH3(C2H4)(1+)*B(C6H3(CF3)2)4(1-)=(C6H3(CH3)2NCCH3)2C5H3NRuCH3(C2H4)*B(C6H3(CF3)2)4 (314733-80-7)

Guidance literature:

In dichloromethane; a mixt. in Ch2Cl2 was stirred for 2h at room temp. under ethylene; filtered, dried in vac., chromy. on Florisil column under Ar (CH2Cl2); the solvent was removed in vac.; elem. anal.;

DOI:10.1021/om000674i

upstream raw materials:

ethene

[2,6-(2,6-Me₂C₆H₃NCMe)2pyridyl]RuCl₂(ethylene)

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

Downstream raw materials:

(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCH₃(C₂H₄)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=(C₆H₃(CH₃)2NCCH₃)2C₅H₃NRuCH₃(C₂H₄)*B(C₆H₃(CF₃)2)4

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