C₄₄H₂₅IN₆Zn

Base Information

Chemical Name:C₄₄H₂₅IN₆Zn
CAS No.:1265365-43-2
Molecular Formula:C₄₄H₂₅IN₆Zn
Molecular Weight:830.017
Hs Code.:

C<sub>44</sub>H<sub>25</sub>IN<sub>6</sub>Zn

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₂₅IN₆Zn

Chemical Property:

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Technology Process of C₄₄H₂₅IN₆Zn

There total 6 articles about C₄₄H₂₅IN₆Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67066-09-5
5-bromo-10,15,20-triphenylporphyrin

: 1265365-43-2
C₄₄H₂₅IN₆Zn

Guidance literature:: Multi-step reaction with 4 steps

1: zinc diacetate / methanol; chloroform / 0.08 h / Heating

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / -196 - 20 °C / Cooling with liquid nitrogen; Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran; dichloromethane / 0.25 h / 20 °C

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; zinc diacetate; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1142/S1088424610002720

Reference yield:

: 162479-04-1
(5-bromo-10,15,20-triphenylporphyrinato)zinc(II)

: 1265365-43-2
C₄₄H₂₅IN₆Zn

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / -196 - 20 °C / Cooling with liquid nitrogen; Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran; dichloromethane / 0.25 h / 20 °C

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane; 1: Sonogashira coupling / 3: Sonogashira coupling;
DOI:10.1142/S1088424610002720

Reference yield:

: 1205553-91-8
C₄₃H₃₂N₄SiZn

: 1265365-43-2
C₄₄H₂₅IN₆Zn

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran; dichloromethane / 0.25 h / 20 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane; 2: Sonogashira coupling;
DOI:10.1142/S1088424610002720