4-Methylphenyl2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-1-thio-β-D-Glucopyranoside

Base Information

Chemical Name:4-Methylphenyl2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-1-thio-β-D-Glucopyranoside
CAS No.:850416-39-6
Molecular Formula:C34H34O5S
Molecular Weight:554.707
Hs Code.:2938909090
Mol file:850416-39-6.mol

Synonyms:4-methyl-(2',2',2'-trifluoroethylthio)benzene;p-Tolyl-2,2,2-trifluorethylsulfid;2,2,2-trifluoroethyl 4-methylphenyl sulfide;p-Methylphenyl-2,2,2-trifluorethyl-sulfid;p-tolyl 2,2,2-trifluoroethyl sulfide;Benzene,1-methyl-4-[(2,2,2-trifluoroethyl)thio];p-tolyl(2,2,2-trifluoroethyl)sulfane;

Suppliers and Price of 4-Methylphenyl2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-1-thio-β-D-Glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 14 raw suppliers

Chemical Property of 4-Methylphenyl2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-1-thio-β-D-Glucopyranoside

Chemical Property:

Melting Point:123-125 °C
Boiling Point:682.4±55.0 °C(Predicted)
PSA：71.45000
Density:1.25±0.1 g/cm3(Predicted)
LogP:7.09700

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Methylphenyl2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-1-thio-β-D-Glucopyranoside

There total 11 articles about 4-Methylphenyl2,3-bis-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-1-thio-β-D-Glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-52-7
benzaldehyde

: 596087-18-2
4-methylphenyl 2,3-di-O-benzyl-1-thio-β-D-glucopyranoside

: 850416-39-6
p-methylphenyl 2,3-di-O-benzyl-4,6-O-(R)-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With vanadyl triflate; In acetonitrile; at 20 ℃; for 14h;
DOI:10.1021/ol051178z

Reference yield: 92.0%

: 100-39-0
benzyl bromide

: 219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 850416-39-6
p-methylphenyl 2,3-di-O-benzyl-4,6-O-(R)-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: 4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 5h;
DOI:10.1021/acs.orglett.0c00732