3-Ethyl-5-methyl-4-(2-chlorophenyl)-2-(2,2-diethoxy-ethoxymethyl)-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

Base Information

• Chemical Name: 3-Ethyl-5-methyl-4-(2-chlorophenyl)-2-(2,2-diethoxy-ethoxymethyl)-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate
• CAS No.: 103094-30-0
• Molecular Formula: C24H32ClNO7
• Molecular Weight: 481.97
• Hs Code.: 2933399090
• Mol file: 103094-30-0.mol

Synonyms:3,5-Pyridinedicarboxylic acid, 4-(2-chlorophenyl)-2-[(2,2-diethoxyethoxy)methyl]-1,4-dihydro-6-methyl-, 3-ethyl 5-methyl ester;

Chemical Property of 3-Ethyl-5-methyl-4-(2-chlorophenyl)-2-(2,2-diethoxy-ethoxymethyl)-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.518
• Boiling Point: 553.084 °C at 760 mmHg
• Flash Point: 288.295 °C
• PSA: 92.32000
• Density: 1.18 g/cm³
• LogP: 4.03550

Purity/Quality:

97% ^*data from raw suppliers

3-ETHYL-5-METHYL-4-(2-CHLOROPHENYL)-2-(2,2-DIETHOXY-ETHOXYMETHYL)-6-METHYL-1,4-DIHYDRO-PYRIDINE-3,5-DIDARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Ethyl-5-methyl-4-(2-chlorophenyl)-2-(2,2-diethoxy-ethoxymethyl)-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

There total 19 articles about 3-Ethyl-5-methyl-4-(2-chlorophenyl)-2-(2,2-diethoxy-ethoxymethyl)-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.9%

ethyl 2-(2-chlorobenzylidene)-4-[(2-phthalimido)ethoxy]acetoacetate (400024-08-0) + methyl 3-aminocrotonate (14205-39-1) → 4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-2-[2-phthalimidoethoxymethyl]-1,4-dihydropyridine (88150-62-3,103094-30-0)

Guidance literature:

With acetic acid; at 25 ℃; Temperature; Large scale;

Reference yield: 87.0%

→ 4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-2-[2-phthalimidoethoxymethyl]-1,4-dihydropyridine (88150-62-3,103094-30-0)

Guidance literature:

In hexane; dichloromethane; at 30 - 35 ℃; for 6h; Purification / work up;

Reference yield: 82.4%

ethyl 2-(2-chlorobenzylidene)-4-[(2-phthalimido)ethoxy]acetoacetate (400024-08-0) + methyl (E)-3-aminocrotonate (14205-39-1) → 4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-2-[2-phthalimidoethoxymethyl]-1,4-dihydropyridine (88150-62-3,103094-30-0)

Guidance literature:

In ethanol; at 90 ℃; for 0.333333h; Temperature; Flow reactor;

upstream raw materials:

2-chloro-benzaldehyde

methyl (E)-3-aminocrotonate

ethyl 4-[2-(phthalimido)ethoxy]acetoacetate

methyl 3-aminocrotonate

Downstream raw materials:

2-({2-[(morpholinosulfonyl)amino]ethoxy}methyl)-4-(2-chlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

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