Technology Process of C38H41NO5S
There total 14 articles about C38H41NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 1) NaH, HMPA / THF
2: m-CPBA / CH2Cl2 / -10 °C
3: Sharpless-Reich reaction
4: m-CPBA / CH2Cl2 / 0 °C
5: 1) NaH, HMPA / THF
6: Sharpless-Reich reaction
7: DEAD, PPh3
8: KOH, aq. EtOH / tetrahydrofuran
9: KH / tetrahydrofuran
With
N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; ethanol; potassium hydride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)91850-1
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 1) NaH, HMPA / THF
2: m-CPBA / CH2Cl2 / -10 °C
3: Sharpless-Reich reaction
4: m-CPBA / CH2Cl2 / 0 °C
5: 1) NaH, HMPA / THF
6: Sharpless-Reich reaction
7: DEAD, PPh3
8: KOH, aq. EtOH / tetrahydrofuran
9: KH / tetrahydrofuran
With
N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; ethanol; potassium hydride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)91850-1
- Guidance literature:
-
Multi-step reaction with 10 steps
1: m-CPBA / CH2Cl2 / -10 °C
2: Sharpless-Reich reaction
3: m-CPBA / CH2Cl2 / 0 °C
4: 1) NaH, HMPA / THF
5: Sharpless-Reich reaction
6: DEAD, PPh3
7: KOH, aq. EtOH / tetrahydrofuran
8: KH / tetrahydrofuran
With
N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; ethanol; potassium hydride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)91850-1