3-FLUORO-D-PHENYLALANINE

Base Information

• Chemical Name: 3-FLUORO-D-PHENYLALANINE
• CAS No.: 2629-54-1
• Molecular Formula: C9H10FNO2
• Molecular Weight: 183.18
• Hs Code.: 29224999
• Mol file: 2629-54-1.mol

Synonyms:DL-3-Fluoro-phe-OH;M-FLUORO-D-PHENYLALANINE;RARECHEM BK PT 0028;DL-3-Fluorophenylalanine;D-3-FLUOROPHE;H-M-FLUORO-D-PHE-OH;3-FLUORO-D-PHE;D-3-FLUOROPHENYLALANINE;查看更多英文别名收起

Chemical Property of 3-FLUORO-D-PHENYLALANINE

Chemical Property:

• Vapor Pressure: 0.000369mmHg at 25°C
• Melting Point: ~240 °C (dec.)
• Refractive Index: 1.555
• Boiling Point: 305 °C at 760 mmHg
• Flash Point: 138.3 °C
• PSA: 63.32000
• Density: 1.293g/cm³
• LogP: 1.48040
• Storage Temp.: Store at RT.

Purity/Quality:

99% ^*data from raw suppliers

3-Fluoro-DL-phenylalanine, 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 37-24/25
• Safety Statements: 22-24/25-37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 3-FLUORO-D-PHENYLALANINE

There total 72 articles about 3-FLUORO-D-PHENYLALANINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

diethyl α-acetamido, α-(3-fluorobenzyl)malonate (380-70-1) → 3-fluorophenylalanine (456-88-2,2629-54-1)

Guidance literature:

With hydrogenchloride; In water; for 18h; Reflux;

DOI:10.1016/j.ejmech.2017.10.031

Reference yield:

3-fluorophenylalanine (456-88-2,2629-54-1) → 3-Fluorocinnamic acid (20595-30-6) + (R)-2-amino-3-(3-fluorophenyl)propionic acid (110117-84-5,2629-54-1)

Guidance literature:

With phenylalanine ammonia-lyase from Pseudozyma antarctica yeast; In aq. buffer; at 30 ℃; for 168h; pH=8.5; Reagent/catalyst; Time; stereoselective reaction; Resolution of racemate;

DOI:10.1016/j.cattod.2020.04.002

Reference yield:

(+/-)-3-amino-3-(3-fluorophenyl)propanoic acid (117391-51-2,723284-81-9) → (R)-3-amino-3-(3-fluoro-phenyl)-propionic acid (723284-81-9) + 3-Fluorocinnamic acid (20595-30-6) + L-3-fluorophenylalanine (19883-77-3,2629-54-1)

Guidance literature:

With phenylalanine 2,3-aminomutase from Pantoea agglomerans; ammonium carbonate; at 20 ℃; for 20h; pH=8; enantioselective reaction; Enzymatic reaction;

DOI:10.1039/c6ra02964g

upstream raw materials:

N-acetyl-3-fluoro-L-phenylalanine-(N'-phenyl-hydrazide)

glycine

m-fluorobenzyl chloride

(R,S)-N-phenylacetyl-3-fluorophenylalanine

Downstream raw materials:

N-Boc-3-fluoro-L-phenylalanine

3-fluorophenylalanine

3-(3-fluoro-phenyl)-2-oxo-propionic acid

(S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(3-fluorophenyl)propanoic acid

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