trimesitylgermylcarbodiimide

Base Information

Chemical Name:trimesitylgermylcarbodiimide
CAS No.:261919-37-3
Molecular Formula:C₂₈H₃₄GeN₂
Molecular Weight:471.181
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimesitylgermylcarbodiimide

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Technology Process of trimesitylgermylcarbodiimide

There total 2 articles about trimesitylgermylcarbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 261919-36-2
bis(trimesitylgermylcarbodiimido)germylene

: 7732-18-5
water

: 261919-37-3
trimesitylgermylcarbodiimide

: 12024-99-6
Ge(OH)2

Guidance literature:: In benzene; hydrolysis of Ge compd. in benzene soln. at room temp. in open flask; crystals deposited on vessel walls near liq. surface; elem. anal.;
DOI:10.1016/S0022-328X(99)00577-X

Reference yield: 31.0%

: 1020-31-1,122983-47-5,881376-69-8
3,5-Di-tert-butylcatechol

: 261919-36-2
bis(trimesitylgermylcarbodiimido)germylene

: 261919-37-3
trimesitylgermylcarbodiimide

: 110577-20-3
2-germylene(6,8-di-t-butyl)-4,5-benzo-1,3-dioxolane

: 212907-09-0
trimesitylgermylcyanamide

Guidance literature:: In tetrahydrofuran; under N2 or Ar; soln. of 3,5-di-t-butylcatechol in THF added dropwise with stirring to Ge compd. (molar ratio 1:1) in THF; 4 h at room temp.; total yield of trimesitylgermylcyanamide and trimesitylgermylcarbodiimidewas 69%; solvent evapd. under vac.;
DOI:10.1016/S0022-328X(99)00577-X

Reference yield: 78.0%

: 261919-37-3
trimesitylgermylcarbodiimide

: 212907-09-0
trimesitylgermylcyanamide

: 212907-10-3
bis(trimesitylgermyl)carbodiimide

: 127099-85-8,780722-26-1,461-58-5
N-Cyanoguanidine

Guidance literature:: In chloroform-d1; under N2 or Ar; soln. of Ge compd. in CDCl3 warmed to 80°C for 18 h; ppt. of dicyanamide collected; remaining soln. evapd. under vac.; monitored by (1)H NMR spectra;
DOI:10.1016/S0022-328X(99)00577-X