bis(trimesitylgermyl)carbodiimide

Base Information

Chemical Name:bis(trimesitylgermyl)carbodiimide
CAS No.:212907-10-3
Molecular Formula:C₅₅H₆₆Ge₂N₂
Molecular Weight:900.322
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(trimesitylgermyl)carbodiimide

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Technology Process of bis(trimesitylgermyl)carbodiimide

There total 8 articles about bis(trimesitylgermyl)carbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 261919-37-3
trimesitylgermylcarbodiimide

: 212907-09-0
trimesitylgermylcyanamide

: 212907-10-3
bis(trimesitylgermyl)carbodiimide

: 127099-85-8,780722-26-1,461-58-5
N-Cyanoguanidine

Guidance literature:: In chloroform-d1; under N2 or Ar; soln. of Ge compd. in CDCl3 warmed to 80°C for 18 h; ppt. of dicyanamide collected; remaining soln. evapd. under vac.; monitored by (1)H NMR spectra;
DOI:10.1016/S0022-328X(99)00577-X

Reference yield: 75.0%

: 62120-68-7
chlorotri(2,4,6-trimethylphenyl)germane

: 420-04-2
CYANAMID

: 212907-10-3
bis(trimesitylgermyl)carbodiimide

Guidance literature:: With t-BuLi; In tetrahydrofuran; pentane; byproducts: LiCl; N2-atmosphere; addn. of 2 equiv. of t-BuLi (in pentane) to cyanamide (inTHF) at -65°C, warming to room temp. after 30 min, addn. of 2 eq uiv. of Ge-compd., warming (55°C, 2 h); evapn., dissoln. in C6H6, centrifugation off of LiCl, evapn. (vac.), recrystn. (ether);
DOI:10.1016/S0022-328X(98)00546-4

Reference yield: 64.0%

: 261919-37-3
trimesitylgermylcarbodiimide

: 62120-68-7
chlorotri(2,4,6-trimethylphenyl)germane

: 212907-09-0
trimesitylgermylcyanamide

: 212907-10-3
bis(trimesitylgermyl)carbodiimide

Guidance literature:: With triethyl amine; In tetrahydrofuran; byproducts: (C2H5)3N*HCl; under N2 or Ar; Et3N added to mixt. of Mes3GeNCNH and Mes3GeCl (molar ratio 1:1:1) at room temp. with stirring; 3 h; THF replaced by benzene; centrifuged; soln. evapd. under vac.;
DOI:10.1016/S0022-328X(99)00577-X