trimesitylgermylcyanamide

Base Information

Chemical Name:trimesitylgermylcyanamide
CAS No.:212907-09-0
Molecular Formula:C₂₈H₃₄GeN₂
Molecular Weight:471.181
Hs Code.:

Synonyms:

Suppliers and Price of trimesitylgermylcyanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimesitylgermylcyanamide

Chemical Property:

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Technology Process of trimesitylgermylcyanamide

There total 4 articles about trimesitylgermylcyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1020-31-1,122983-47-5,881376-69-8
3,5-Di-tert-butylcatechol

: 261919-36-2
bis(trimesitylgermylcarbodiimido)germylene

: 261919-37-3
trimesitylgermylcarbodiimide

: 110577-20-3
2-germylene(6,8-di-t-butyl)-4,5-benzo-1,3-dioxolane

: 212907-09-0
trimesitylgermylcyanamide

Guidance literature:: In tetrahydrofuran; under N2 or Ar; soln. of 3,5-di-t-butylcatechol in THF added dropwise with stirring to Ge compd. (molar ratio 1:1) in THF; 4 h at room temp.; total yield of trimesitylgermylcyanamide and trimesitylgermylcarbodiimidewas 69%; solvent evapd. under vac.;
DOI:10.1016/S0022-328X(99)00577-X

Reference yield:

: 261919-37-3
trimesitylgermylcarbodiimide

: 212907-09-0
trimesitylgermylcyanamide

Guidance literature:: With nitromethane; In chloroform; under N2 or Ar; nitromethane added to soln. of Ge compd. in CHCl3; equilibrium between Ge educt and product in soln.; monitored by IR spectra;
DOI:10.1016/S0022-328X(99)00577-X

Reference yield:

: 261919-36-2
bis(trimesitylgermylcarbodiimido)germylene

: 212907-09-0
trimesitylgermylcyanamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: nitromethane / chloroform-d1

With nitromethane; In chloroform-d1; benzene;
DOI:10.1016/S0022-328X(99)00577-X