DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester

Base Information

• Chemical Name: DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester
• CAS No.: 20051-96-1
• Molecular Formula: C₁₆H₂₃NO₃
• Molecular Weight: 277.364
• Mol file: 20051-96-1.mol

Synonyms:

Chemical Property of DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester

There total 3 articles about DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenylalanine (150-30-1,25191-15-5,658-69-5,67675-33-6) → DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester (20051-96-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / diethyl ether

2: SOCl₂ / Heating

With sodium hydroxide; thionyl chloride; In diethyl ether;

DOI:10.1248/cpb.15.1948

Reference yield:

pivaloyl chloride (3282-30-2) → DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester (20051-96-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / diethyl ether

2: SOCl₂ / Heating

With sodium hydroxide; thionyl chloride; In diethyl ether;

DOI:10.1248/cpb.15.1948

Reference yield:

ethanol (64-17-5) + N-(2,2-Dimethylpropanoyl)phenylalanin (19881-88-0) → DL-2-Pivaloylamino-3-phenyl-propionsaeure-aethylester (20051-96-1)

Guidance literature:

With thionyl chloride; Heating;

DOI:10.1248/cpb.15.1948

upstream raw materials:

ethanol

N-(2,2-Dimethylpropanoyl)phenylalanin

Phenylalanine

pivaloyl chloride

Downstream raw materials:

DL-N-<α-Hydroxymethyl-phenethyl>-pivalinsaeureamid