4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one

Base Information

Chemical Name:4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one
CAS No.:105426-92-4
Molecular Formula:C₃₁H₅₀O₇
Molecular Weight:534.734
Hs Code.:

Synonyms:

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Chemical Property of 4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one

Chemical Property:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one

There total 15 articles about 4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4179-00-4
Methyl (E)-3-methyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2-pentenoate

: 105426-92-4
4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one

Guidance literature:: Multi-step reaction with 10 steps

1: lithium aluminium hydride

2: PBr₃ / pyridine

4: 2N HCl / 0.05 h / 0 °C

6: 95 percent / diisobutylaluminium hydride / CH₂Cl₂

7: DMAP, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

8: LiCl / dimethylformamide / 0.5 h / 0 °C

10: O₂, rose bengal / CH₂Cl₂; methanol / -78 °C / Irradiation

With hydrogenchloride; dmap; lithium aluminium tetrahydride; oxygen; phosphorus tribromide; rose bengal; diisobutylaluminium hydride; triethylamine; lithium chloride; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)98937-8

Reference yield:

: 18665-81-1
(E)-3-methyl-5-(2',6',6'-trimethylcyclohex-1'-en-1'-yl)pent-2-en-1-ol

: 105426-92-4
4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one

Guidance literature:: Multi-step reaction with 9 steps

1: PBr₃ / pyridine

3: 2N HCl / 0.05 h / 0 °C

5: 95 percent / diisobutylaluminium hydride / CH₂Cl₂

6: DMAP, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

7: LiCl / dimethylformamide / 0.5 h / 0 °C

9: O₂, rose bengal / CH₂Cl₂; methanol / -78 °C / Irradiation

With hydrogenchloride; dmap; oxygen; phosphorus tribromide; rose bengal; diisobutylaluminium hydride; triethylamine; lithium chloride; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)98937-8

Reference yield:

: 29550-53-6
(E)-3-methyl-5-(2',6',6'-trimethylcyclohex-1'-enyl)pent-2-enyl bromide

: 105426-92-4
4-[(3Z,7E)-4-Dimethoxymethyl-1-(1-ethoxy-ethoxy)-8-methyl-10-(2,6,6-trimethyl-cyclohex-1-enyl)-deca-3,7-dienyl]-5-hydroxy-5H-furan-2-one

Guidance literature:: Multi-step reaction with 8 steps

2: 2N HCl / 0.05 h / 0 °C

4: 95 percent / diisobutylaluminium hydride / CH₂Cl₂

5: DMAP, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

6: LiCl / dimethylformamide / 0.5 h / 0 °C

8: O₂, rose bengal / CH₂Cl₂; methanol / -78 °C / Irradiation

With hydrogenchloride; dmap; oxygen; rose bengal; diisobutylaluminium hydride; triethylamine; lithium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)98937-8