2,2,5,5-Tetrakis-trimethylsilanyl-silolane

Base Information

• Chemical Name: 2,2,5,5-Tetrakis-trimethylsilanyl-silolane
• CAS No.: 124080-35-9
• Molecular Formula: C₁₆H₄₂Si₅
• Molecular Weight: 374.937
• Mol file: 124080-35-9.mol

Synonyms:

Chemical Property of 2,2,5,5-Tetrakis-trimethylsilanyl-silolane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,5,5-Tetrakis-trimethylsilanyl-silolane

There total 1 articles about 2,2,5,5-Tetrakis-trimethylsilanyl-silolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

[((C6H11)3PPd)2(SiC4H4(Si(CH3)3)4)] + hydrogen (1333-74-0) → palladium(0)bis(tricyclohexylphosphine) (33309-88-5) + 2,2,5,5-Tetrakis-trimethylsilanyl-silolane (124080-35-9)

Guidance literature:

In benzene-d6; byproducts: Pd; complex reacted slowly with excess of H2 under atm. pressure in C6D6;

DOI:10.1246/cl.2007.284

Reference yield: 86.0%

2,2,5,5-Tetrakis-trimethylsilanyl-silolane (124080-35-9) + benzyl azide (622-79-7) → C23H47NSi5 (1246071-72-6)

Guidance literature:

In hexane; at 20 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1039/c0nj00121j

Reference yield: 77.0%

2,2,5,5-Tetrakis-trimethylsilanyl-silolane (124080-35-9) + Phenyl azide (622-37-7) → C22H45NSi5 (1246071-73-7)

Guidance literature:

In hexane; at 20 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1039/c0nj00121j

upstream raw materials:

hydrogen

Downstream raw materials:

C₂₃H₄₇NSi₅

C₂₂H₄₅NSi₅