[Li(OB(mesityl)2)(Et₂O)]2

Base Information

Chemical Name:[Li(OB(mesityl)2)(Et₂O)]2
CAS No.:794589-75-6
Molecular Formula:C₄₄H₆₄B₂Li₂O₄
Molecular Weight:692.494
Hs Code.:

Synonyms:

Suppliers and Price of [Li(OB(mesityl)2)(Et₂O)]2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [Li(OB(mesityl)2)(Et₂O)]2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [Li(OB(mesityl)2)(Et₂O)]2

There total 1 articles about [Li(OB(mesityl)2)(Et₂O)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 60-29-7,927820-24-4
diethyl ether

: 20631-84-9
dimesitylborinic acid

: 794589-75-6
[Li(OB(mesityl)2)(Et₂O)]2

Guidance literature:: In tetrahydrofuran; hexane; (N2); addn. of a soln. of lithium compd. in hexanes to a soln. of boron compd. in THF at 0°C, warming to room temp., stirring for 1 h, evapn., dissolving in Et2O; storge at room temp.; elem. anal.;
DOI:10.1021/om049520j

Reference yield: 60.0%

: 794589-75-6
[Li(OB(mesityl)2)(Et₂O)]2

: magnesium bromide ethyl etherate

: Mg(OB(mesityl)2)Br*LiBr

Guidance literature:: In diethyl ether; (N2); addn. of lithium complex to a soln. of magnesium compd. in Et2O, stirring for 14 h at room temp.; evapn., extn. with Et2O, concn., storage at -30°C; elem. anal.;
DOI:10.1021/om049520j

Reference yield: 30.0%

: 794589-75-6
[Li(OB(mesityl)2)(Et₂O)]2

: 676-58-4
methylmagnesium chloride

: 794589-80-3
[Mg(OB(mesityl)2)Me(THF)]2

Guidance literature:: In tetrahydrofuran; diethyl ether; byproducts: LiCl; (N2); addn. of lithium complex to a soln. of magnesium compd. in THF at -78°C, diln. with Et2O, stirring for 14 h at room temp.; evapn., extn. with toluene at 100°C, concn., storage at 4°C;
DOI:10.1021/om049520j