C₁₅⁽¹³⁾C₂H₂₆N₂O₅

Base Information

• Chemical Name: C₁₅⁽¹³⁾C₂H₂₆N₂O₅
• CAS No.: 106334-47-8
• Molecular Formula: C₁₇H₂₆N₂O₅
• Molecular Weight: 340.382
• Mol file: 106334-47-8.mol

Synonyms:

Chemical Property of C₁₅⁽¹³⁾C₂H₂₆N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅⁽¹³⁾C₂H₂₆N₂O₅

There total 5 articles about C₁₅⁽¹³⁾C₂H₂₆N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile (58632-95-4) → C15(13)C2H26N2O5 (106334-47-8)

Guidance literature:

Multi-step reaction with 5 steps

1: Et₃N / acetone; H₂O

2: KHCO₃ / dimethylformamide

3: 1.) LDA / 1.) THF, -78 deg C, 2.) HOAc

4: H₂ / Pd(OH)2/C / ethanol

5: DCC, HOBT / ethyl acetate

With hydrogen; benzotriazol-1-ol; potassium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; palladium dihydroxide; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide; acetone;

DOI:10.1016/S0040-4039(00)84644-4

Reference yield:

2-((tert-butoxycarbonyl)amino)-(1-13C)acetic acid (97352-64-2) → C15(13)C2H26N2O5 (106334-47-8)

Guidance literature:

Multi-step reaction with 4 steps

1: KHCO₃ / dimethylformamide

2: 1.) LDA / 1.) THF, -78 deg C, 2.) HOAc

3: H₂ / Pd(OH)2/C / ethanol

4: DCC, HOBT / ethyl acetate

With hydrogen; benzotriazol-1-ol; potassium hydrogencarbonate; dicyclohexyl-carbodiimide; lithium diisopropyl amide; palladium dihydroxide; In ethanol; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)84644-4

Reference yield:

N-BOC-glycine-1-(13)C benzyl ester (106334-45-6) → C15(13)C2H26N2O5 (106334-47-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -78 deg C, 2.) HOAc

2: H₂ / Pd(OH)2/C / ethanol

3: DCC, HOBT / ethyl acetate

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; lithium diisopropyl amide; palladium dihydroxide; In ethanol; ethyl acetate;

DOI:10.1016/S0040-4039(00)84644-4

upstream raw materials:

N-benzyloxyamine

2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

2-((tert-butoxycarbonyl)amino)-(1-¹³C)acetic acid

N-BOC-glycine-1-⁽¹³⁾C benzyl ester

Refernces