tungsten oxytetrachloride

Base Information

Chemical Name:tungsten oxytetrachloride
CAS No.:160797-03-5
Molecular Formula:Cl₄OW
Molecular Weight:341.661
Hs Code.:

Synonyms:

Suppliers and Price of tungsten oxytetrachloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tungsten oxytetrachloride

Chemical Property:

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Technology Process of tungsten oxytetrachloride

There total 22 articles about tungsten oxytetrachloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 107-46-0
Hexamethyldisiloxane

: 13283-01-7
tungsten(VI) chloride

: 160797-03-5,13520-78-0
tungsten oxytetrachloride

Guidance literature:: In dichloromethane; byproducts: Me3SiCl; under inert atm.; soln. of Si-compd. added dropwise to a stirred suspension of W-compd. at room temp. over a period of 15 min, deposition of crystals, mixt. stirred at room temp. for 60 min; supernatant decanted, solid collected, washed (petroleum ether), dried (vac.); elem. anal.;
DOI:10.1016/S0277-5387(00)86956-9

Reference yield: 96.49%

: 13283-01-7
tungsten(VI) chloride

: 67-64-1
acetone

: 13520-78-0,160797-03-5
tungsten(VI) oxychloride

Guidance literature:: In n-heptane; at 19 - 30 ℃; for 3.5h; Solvent; Temperature;

Reference yield: 95.3%

: 76-06-2
chloropicrin

: 13283-01-7
tungsten(VI) chloride

: 13520-78-0,160797-03-5
tungsten(VI) oxychloride

Guidance literature:: In neat (no solvent); byproducts: NOCl, CCl4; under exclusion of moisture, refluxed for 10 min, cooled quickly to 0°C; filtered; dried under vac.; elem. anal.;