diacetoxytriphenylarsorane

Base Information

• Chemical Name: diacetoxytriphenylarsorane
• CAS No.: 50289-98-0
• Molecular Formula: C₂₂H₂₁AsO₄
• Molecular Weight: 424.328
• Mol file: 50289-98-0.mol

Synonyms:

Chemical Property of diacetoxytriphenylarsorane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diacetoxytriphenylarsorane

There total 4 articles about diacetoxytriphenylarsorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

triphenyl-arsane (603-32-7) + [bis(acetoxy)iodo]benzene (3240-34-4) → diacetoxytriphenylarsorane (50289-98-0)

Guidance literature:

In chloroform-d1; for 24h; Inert atmosphere; Glovebox;

DOI:10.1039/d0dt00777c

Reference yield: 74.0%

triphenylarsenic dichloride (2526-65-0) + acetic acid (64-19-7,77671-22-8) → diacetoxytriphenylarsorane (50289-98-0)

Guidance literature:

With triethylamine; In benzene; for 1h; Ambient temperature;

Reference yield:

N-(p-bromophenyl)triphenylarsine imide (110788-31-3) → diacetoxytriphenylarsorane (50289-98-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / benzene

2: 74 percent / Et₃N / benzene / 1 h / Ambient temperature

With triethylamine; In benzene;

upstream raw materials:

triphenylarsenic dichloride

acetic acid

triphenylarsenazophenyl

N-(p-bromophenyl)triphenylarsine imide

Downstream raw materials:

N-(2,2,t-3,4,4-pentamethylphosphetan-r-1-yl)triphenylarsoranylideneamine P-oxide

N-(di-isopropylphosphinoyl)triphenylarsoranylideneamine

N-(di-t-butylphosphinoyl)triphenylarsoranylideneamine