1-Bromo-3-chloro-4-(methylthio)benzene

Base Information

• Chemical Name: 1-Bromo-3-chloro-4-(methylthio)benzene
• CAS No.: 101084-82-6
• Molecular Formula: C7H6BrClS
• Molecular Weight: 237.548
• Mol file: 101084-82-6.mol

Synonyms:<4-Brom-2-chlor-phenyl>-methyl-sulfid;2-Chlor-4-brom-thioanisol;4-bromo-2-chloro-1-methylsulfanyl benzene;4-bromo-2-chloro-1-(methylthio)benzene;2-CHLORO-4-BROMO THIOANISOLE;

Chemical Property of 1-Bromo-3-chloro-4-(methylthio)benzene

Chemical Property:

• PSA: 25.30000
• LogP: 3.82440

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-Bromo-3-chloro-4-(methylthio)benzene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Bromo-3-chloro-4-(methylthio)benzene

There total 4 articles about 1-Bromo-3-chloro-4-(methylthio)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-bromo-2-chlorobenzenethiol (99839-25-5) + methyl iodide (74-88-4) → 4-bromo-2-chloro-1-(methylsulfanyl)benzene (101084-82-6)

Guidance literature:

With potassium carbonate; In acetone; at 20 ℃;

Reference yield: 92.0%

1-bromo-3-chloro-4-fluorobenzene (60811-21-4) + sodium thiomethoxide (5188-07-8) → 4-bromo-2-chloro-1-(methylsulfanyl)benzene (101084-82-6)

Guidance literature:

In water; N,N-dimethyl-formamide; at 50 ℃; for 2h;

Reference yield: 87.0%

1-chloromethyl-2-methylsulfanylbenzene (26190-68-1) → 4-bromo-2-chloro-1-(methylsulfanyl)benzene (101084-82-6)

Guidance literature:

With bromine; iron; In dichloromethane; for 2h;

upstream raw materials:

1-chloromethyl-2-methylsulfanylbenzene

1-bromo-3-chloro-4-fluorobenzene

sodium thiomethoxide

4-bromo-2-chlorobenzenethiol

Downstream raw materials:

Toluene-4-sulfonic acid 1-(3-chloro-4-methylsulfanyl-phenyl)-2,2-dimethyl-propyl ester

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