p-(ethoxycarbonyl)phenylselenotrimethylstannane

Base Information

Chemical Name:p-(ethoxycarbonyl)phenylselenotrimethylstannane
CAS No.:284043-22-7
Molecular Formula:C₁₂H₁₈O₂SeSn
Molecular Weight:391.944
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-(ethoxycarbonyl)phenylselenotrimethylstannane

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Technology Process of p-(ethoxycarbonyl)phenylselenotrimethylstannane

There total 1 articles about p-(ethoxycarbonyl)phenylselenotrimethylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1066-45-1
trimethyltin(IV)chloride

: 181075-86-5
bis(p-(ethoxycarbonyl)phenyl)diselenide

: 284043-22-7
p-(ethoxycarbonyl)phenylselenotrimethylstannane

Guidance literature:: With NaBH₄; In tetrahydrofuran; ethanol; bis(p-ethoxycarbonyl)phenyldiselenide suspended in EtOH under stirring at room temp. and Ar, reduced by addition of small portions of NaBH4, stirred, a soln. Me3SnCl in THF added, stirred for 30 min, mixt. taken up with water, extracted with CHCl3; extract washed with water, dried (Na2SO4), product purified by column chromy.;
DOI:10.1002/(SICI)1099-0682(200006)2000:6<1307::AID-EJIC1307>3.3.CO;2-Q

Reference yield: 98.0%

: 13709-36-9
xenon difluoride

: 284043-22-7
p-(ethoxycarbonyl)phenylselenotrimethylstannane

: 928-49-4
hex-3-yne

: 420-60-0
trimethyltin fluoride

: 181075-89-8
(E)-3-[(p-ethoxycarbonyl)phenylseleno]-4-fluorohex-3-ene

Guidance literature:: In dichloromethane; XeF2 added in small portions under Ar to a soln. of selenide in CH2Cl2 at -20°C, stirred for 30 min, the acetylene added, stirred for 1 h at -20°C and for 1 h at room temp.; precipitate separated, washed with n-pentane, solvent removed under vacuum, crude product purified by column chromy., elem. anal.;
DOI:10.1002/(SICI)1099-0682(200006)2000:6<1307::AID-EJIC1307>3.3.CO;2-Q