Bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate

Base Information

Chemical Name:Bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate
CAS No.:866-05-7
Molecular Formula:C15H6 F24 O3
Molecular Weight:690.173
Hs Code.:
NSC Number:86761
DSSTox Substance ID:DTXSID40293010
Wikidata:Q82031556

Synonyms:866-05-7;bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate;Bis(1H,1H,7H-perfluoroheptyl) carbonate;NSC86761;DTXSID40293010;NSC-86761;CS-0459271

Suppliers and Price of Bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate

Chemical Property:

Vapor Pressure:0.001mmHg at 25°C
Boiling Point:302.2°C at 760 mmHg
Flash Point:132.3°C
Density:1.651g/cm³
XLogP3:8.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:27
Rotatable Bond Count:16
Exact Mass:689.9933699
Heavy Atom Count:42
Complexity:881

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(C(C(C(C(C(C(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)OC(=O)OCC(C(C(C(C(C(F)F)(F)F)(F)F)(F)F)(F)F)(F)F

Technology Process of Bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate

There total 2 articles about Bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-09-0
bis(phenyl) carbonate

: tetrabutoxytitanium

: 335-99-9
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol

: 542-52-9
Dibutyl carbonate

: 866-05-7
bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate

: C₁₂H₁₂F₁₂O₃

Guidance literature:: tetrabutoxytitanium; 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol; Heating; Green chemistry;

bis(phenyl) carbonate; Overall yield = 67 percent; Green chemistry;
DOI:10.1016/j.mencom.2021.03.038

Reference yield:

: 56-23-5
tetrachloromethane

: 335-99-9
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol

: 424-07-7
1-chloro-1H,1H,7H-perfluoroheptane

: 866-05-7
bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate

: 866-92-2
(1,1,7-Trihydro-perfluor-heptyl)-orthocarbonat

Guidance literature:: iron(III) chloride;
DOI:10.1021/jo01013a025

Reference yield:

: 866-05-7
bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl) carbonate

: 1550-24-9
7-Chlor-perfluorheptansaeure

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂ / Irradiation

2: 165 - 225 °C

3: H₂O

With water; chlorine;
DOI:10.1021/jo01070a074