C₂N₂H₂(mesityl)2SbCl

Base Information

• Chemical Name: C₂N₂H₂(mesityl)2SbCl
• CAS No.: 811470-79-8
• Molecular Formula: C₂₀H₂₄ClN₂Sb
• Molecular Weight: 449.627
• Mol file: 811470-79-8.mol

Synonyms:

Chemical Property of C₂N₂H₂(mesityl)2SbCl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₂N₂H₂(mesityl)2SbCl

There total 1 articles about C₂N₂H₂(mesityl)2SbCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

(CH3)3C6H2NC2H3NHC6H2(CH3)3 + chlorobis(dimethylamino)stibane (95688-59-8) → C2N2H2(mesityl)2SbCl (811470-79-8)

Guidance literature:

In not given;

DOI:10.1039/b409657f

Reference yield: 50.0%

1-chloro-2,3,4,5-tetraethylphosphole (312920-30-2) + C2N2H2(mesityl)2SbCl (811470-79-8) → 1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene (1245505-08-1)

Guidance literature:

With Li; In tetrahydrofuran; Li reacted with phosphole deriv. in THF; soln. added dropwise to cooled (-78°C) soln. of Sb compd. in THF; mixt. allowed to warm to room temp., stirred for 1 h; solvent removed under reduced pressure, dissolved in hexane; ppt. removed by filtration, vol. reduced to 20 mL, stored at -20°C for crystn.; ppt. collected by filtration, dried in vacuo; elem. anal.;

DOI:10.1002/zaac.200900564

Reference yield:

aluminium trichloride (7446-70-0) + C2N2H2(mesityl)2SbCl (811470-79-8) → [(CH3)3C6H2N]2C2H2Sb(1+)*AlCl4(1-)=[(CH3)3C6H2N]2C2H2Sb(AlCl4)

Guidance literature:

In not given; with 1 equiv. of AlCl3;

DOI:10.1039/b409657f

upstream raw materials:

chlorobis(dimethylamino)stibane

Downstream raw materials:

1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene