RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃)⁽¹⁺⁾*PF₆^(1-)=(RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃))PF₆

Base Information

Chemical Name:RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃)⁽¹⁺⁾*PF₆^(1-)=(RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃))PF₆
CAS No.:145312-34-1
Molecular Formula:C₂₅H₂₇ClOPRuS₃*F₆P
Molecular Weight:752.148
Hs Code.:

RuCl(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>6</sub>H<sub>12</sub>S<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(RuCl(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>6</sub>H<sub>12</sub>S<sub>3</sub>))PF<sub>6</sub>

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Chemical Property of RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃)⁽¹⁺⁾*PF₆^(1-)=(RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃))PF₆

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Technology Process of RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃)⁽¹⁺⁾*PF₆^(1-)=(RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃))PF₆

There total 3 articles about RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃)⁽¹⁺⁾*PF₆^(1-)=(RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃))PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: ammonium hexafluorophosphate

: 25360-32-1,22337-78-6
carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II)

: 6573-11-1
1,4,7-trithiacyclononane

: 145312-34-1
RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃)⁽¹⁺⁾*PF₆^(1-)=(RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃))PF₆

Guidance literature:: In dichloromethane; react. of Os-complex with (9)aneS3 in refluxing CH2Cl2 under N2 for 15 h (yellow soln.), evapn. (reduced pressure), dissoln. of residue in hot EtOH, addn. of excess NH4PF6 in H2O (yellow ppt.); collection, washing with EtOH and Et2O, drying in vac.; elem. anal.;
DOI:10.1039/DT9920002977

Reference yield: 82.0%

: ammonium hexafluorophosphate

: 6573-11-1
1,4,7-trithiacyclononane

: Ru⁽²⁺⁾*2Cl^(1-)*CO*(CH₃)2NCHO*P(C₆H₅)3=RuCl₂(CO)(P(C₆H₅)3)((CH₃)2NCHO)

: 145312-34-1
RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃)⁽¹⁺⁾*PF₆^(1-)=(RuCl(CO)(P(C₆H₅)3)(C₆H₁₂S₃))PF₆

Guidance literature:: In ethanol; water; react. of Os-complex with (9)aneS3 in refluxing EtOH for 10 min (pale yelow soln.), addn. of excess NH4PF6 in H2O (yellow ppt.); collection, washing with EtOH and Et2O, drying in vac.;
DOI:10.1039/DT9920002977