Stannane, iodomethyldiphenyl-

Base Information

• Chemical Name: Stannane, iodomethyldiphenyl-
• CAS No.: 1015-39-0
• Molecular Formula: C13H13ISn
• Molecular Weight: 414.861
• Mol file: 1015-39-0.mol

Synonyms:

Chemical Property of Stannane, iodomethyldiphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Stannane, iodomethyldiphenyl-

There total 13 articles about Stannane, iodomethyldiphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

triphenyl methyl tin (1089-59-4) + iodine (7553-56-2,12190-71-5,8031-47-8) → methyldiphenyltin(IV) iodide (1015-39-0)

Guidance literature:

In dichloromethane; I2 added in small portions to the stannane in CH2Cl2, stirred for 20 min; concd., distilled under vac.; elem. anal.;

DOI:10.1039/b200317c

Reference yield: 62.0%

triphenyl methyl tin (1089-59-4) → methyldiphenyltin(IV) iodide (1015-39-0)

Guidance literature:

In dichloromethane; to soln. of MePh3Sn in CH2Cl2 soln. of I2 in CH2Cl2 was added at 0°C, mixt. was stirred for 10 h at room temp. (N2); evapd., crystd. from hexane at -78°C; elem. anal.;

DOI:10.1021/om00126a014

Reference yield:

iodotriphenylstannane (894-09-7) → methyldiphenyltin(IV) iodide (1015-39-0)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₃MgI / diethyl ether

2: I₂ / ethanol

With CH₃MgI; I₂; In diethyl ether; ethanol;

upstream raw materials:

triphenyl methyl tin

iodine

bis(triphenyltin) sulfide

diphenylstannane

Downstream raw materials:

benzyldiphenylmethyltin

(-)-(2-phenylbutyl)methyldiphenyltin

(E)-cinnamyl(methyl)diphenylstannane