C₂₇H₂₉FN₂O

Base Information

Chemical Name:C₂₇H₂₉FN₂O
CAS No.:1409968-55-3
Molecular Formula:C₂₇H₂₉FN₂O
Molecular Weight:416.538
Hs Code.:

C<sub>27</sub>H<sub>29</sub>FN<sub>2</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₉FN₂O

Chemical Property:

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Technology Process of C₂₇H₂₉FN₂O

There total 7 articles about C₂₇H₂₉FN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1126-09-6
4-carbethoxypiperidine

: 1409968-55-3
C₂₇H₂₉FN₂O

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / tetrahydrofuran; water

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

2.2: 20 °C

3.1: sodium azide / N,N-dimethyl-formamide / 90 °C

4.1: 10% Pd/C; hydrogen / ethanol

5.1: trifluoroacetic acid / dichloromethane

6.1: potassium carbonate / N,N-dimethyl-formamide

7.1: sodium hydride; sodium iodide / N,N-dimethyl-formamide

With sodium azide; 10% Pd/C; hydrogen; sodium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.09.035

Reference yield:

: 212782-43-9
1-tert-butyl 4-ethyl 4-(2-chloroethyl)piperidine-1,4-dicarboxylate

: 1409968-55-3
C₂₇H₂₉FN₂O

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / N,N-dimethyl-formamide / 90 °C

2: 10% Pd/C; hydrogen / ethanol

3: trifluoroacetic acid / dichloromethane

4: potassium carbonate / N,N-dimethyl-formamide

5: sodium hydride; sodium iodide / N,N-dimethyl-formamide

With sodium azide; 10% Pd/C; hydrogen; sodium hydride; potassium carbonate; trifluoroacetic acid; sodium iodide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.09.035

Reference yield:

: 268550-48-7
1-oxo-2,8-diaza-spiro[4.5]decane-8-carboxylic acid tert-butyl ester

: 1409968-55-3
C₂₇H₂₉FN₂O

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane

2: potassium carbonate / N,N-dimethyl-formamide

3: sodium hydride; sodium iodide / N,N-dimethyl-formamide

With sodium hydride; potassium carbonate; trifluoroacetic acid; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.09.035