Ph₃SnInBr₂ N,N,N',N'-tetramethylethanediamine adduct

Base Information

• Chemical Name: Ph₃SnInBr₂ N,N,N',N'-tetramethylethanediamine adduct
• CAS No.: 113529-46-7
• Molecular Formula: C₂₄H₃₁Br₂InN₂Sn
• Molecular Weight: 740.862
• Mol file: 113529-46-7.mol

Synonyms:

Chemical Property of Ph₃SnInBr₂ N,N,N',N'-tetramethylethanediamine adduct

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ph₃SnInBr₂ N,N,N',N'-tetramethylethanediamine adduct

There total 1 articles about Ph₃SnInBr₂ N,N,N',N'-tetramethylethanediamine adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

indium(I) bromide + N,N,N,N,-tetramethylethylenediamine (110-18-9) + triphenyltin bromide (962-89-0) → Ph3SnInBr2 N,N,N',N'-tetramethylethanediamine adduct (113529-46-7)

Guidance literature:

In toluene; The suspn. of InX and Ph3SnX in toluene was cooled to -20°C, diamine was added stirring was continued for about 1 h; allowed to warm to room temp. for 1-2 h (N2 atm.);; filtered, solid was washed with toluene and dried in vac. at room temp.; elem. anal.;;

DOI:10.1016/0022-328X(87)80390-X

Reference yield:

Ph3SnInBr2 N,N,N',N'-tetramethylethanediamine adduct (113529-46-7) + ethylene dibromide (106-93-4) → InBr2*1.5(C6H16N2) + triphenyltin bromide (962-89-0)

Guidance literature:

In neat (no solvent); byproducts: C2H4; The suspn. of reagents was stirred at room temp. for 3 h (N2 atm.); filtered, washed with toluene and dried in vac.; elem. anal.;;

DOI:10.1016/0022-328X(87)80390-X

upstream raw materials:

N,N,N,N,-tetramethylethylenediamine

triphenyltin bromide

Downstream raw materials:

triphenyltin bromide