Methoxy(phenyl)[tris(trimethylsilyl)methyl]silanol

Base Information

Chemical Name:Methoxy(phenyl)[tris(trimethylsilyl)methyl]silanol
CAS No.:101973-37-9
Molecular Formula:C₁₇H₃₆O₂Si₄
Molecular Weight:384.814
Hs Code.:
DSSTox Substance ID:DTXSID10577450

Synonyms:101973-37-9;Methoxy(phenyl)[tris(trimethylsilyl)methyl]silanol;DTXSID10577450

Suppliers and Price of Methoxy(phenyl)[tris(trimethylsilyl)methyl]silanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methoxy(phenyl)[tris(trimethylsilyl)methyl]silanol

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:384.17923652
Heavy Atom Count:23
Complexity:364

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CO[Si](C1=CC=CC=C1)(C([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)O

Technology Process of Methoxy(phenyl)[tris(trimethylsilyl)methyl]silanol

There total 3 articles about Methoxy(phenyl)[tris(trimethylsilyl)methyl]silanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 124-41-4
sodium methylate

: 101973-39-1
Iodo-phenyl-(tris-trimethylsilanyl-methyl)-silanol

: 101973-37-9
Methoxy-phenyl-(tris-trimethylsilanyl-methyl)-silanol

Guidance literature:: In methanol; for 0.0833333h; Ambient temperature;
DOI:10.1016/0022-328X(85)87333-2

Reference yield:

: 72190-78-4
[Iodo-(tris-trimethylsilanyl-methyl)-silanyl]-benzene

: 101973-37-9
Methoxy-phenyl-(tris-trimethylsilanyl-methyl)-silanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) H₂O, 2.) AgClO₄, H₂O / 1.) dioxane, reflux, 1 h, 2.) dioxane, reflux, 30 min

2: 94 percent / ICl / CCl₄ / Ambient temperature

3: 89 percent / methanol / 0.08 h / Ambient temperature

With water; silver perchlorate; Iodine monochloride; In methanol; tetrachloromethane;
DOI:10.1016/0022-328X(85)87333-2