2-(2,6-dimethoxyphenyl)benzothiazoline

Base Information

Chemical Name:2-(2,6-dimethoxyphenyl)benzothiazoline
CAS No.:515156-32-8
Molecular Formula:C₁₅H₁₅NO₂S
Molecular Weight:273.356
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,6-dimethoxyphenyl)benzothiazoline

Chemical Property:

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Technology Process of 2-(2,6-dimethoxyphenyl)benzothiazoline

There total 1 articles about 2-(2,6-dimethoxyphenyl)benzothiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 137-07-5
2-amino-benzenethiol

: 3392-97-0
2,6-dimethoxybenzaldehyde

: 515156-32-8
2-(2,6-dimethoxyphenyl)benzothiazoline

Guidance literature:: In ethanol; for 0.5h; Heating;
DOI:10.1246/bcsj.76.127

Reference yield: 64.0%

: 75-09-2
dichloromethane

: 6018-89-9
nickel(II) acetate tetrahydrate

: 515156-32-8
2-(2,6-dimethoxyphenyl)benzothiazoline

: bis[2-(2,6-dimethoxyphenylmethyleneamino)-benzenethiolato]nickel(II)

Guidance literature:: In ethanol; Ni salt and benzothiazoline refluxed in EtOH for 1.5 h, cooled to room temp.; ppt. filtered; elem. anal.;
DOI:10.1246/bcsj.76.127

Reference yield:

: 14694-95-2
Wilkinson's catalyst

: 108-88-3,15644-74-3,16713-13-6
toluene

: 515156-32-8
2-(2,6-dimethoxyphenyl)benzothiazoline

: RhCl(P(C₆H₅)3)2SC₆H₄NCHC₆H₃OCH₃*0.5C₆H₅CH₃

: Rh(P(C₆H₅)3)SC₆H₄NHCH₂C₆H₃(OCH₃)2SC₆H₄NCHOC₆H₃OCH₃*0.75CH₂Cl₂

Guidance literature:: In toluene; 2:1 reaction of organic ligand and Rh-compound in toluene under reflux for 20 min; two Rh-complexes isolated in ca. 1:5 ratio after chromatographic purification, elem. anal.;
DOI:10.1246/cl.2003.1058