1,4-bisbutanediol

Base Information

Chemical Name:1,4-bisbutanediol
CAS No.:222319-96-2
Molecular Formula:C₃₀H₃₀O₁₆
Molecular Weight:646.559
Hs Code.:

1,4-bis<bis(methoxycarbonyl)caffeoyl>butanediol

Synonyms:

Suppliers and Price of 1,4-bisbutanediol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-bisbutanediol

Chemical Property:

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Technology Process of 1,4-bisbutanediol

There total 3 articles about 1,4-bisbutanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 331-39-5,501-16-6
caffeic acid

: 222319-96-2
1,4-bisbutanediol

Guidance literature:: Multi-step reaction with 3 steps

1: 1N aq. NaOH / 0 °C

2: thionyl chloride / 80 - 90 °C

3: 0.25 h / 130 - 140 °C

With sodium hydroxide; thionyl chloride;
DOI:10.1021/jm9804735

Reference yield:

: 18959-40-5
3,4-O-dimethoxycarbonyl caffeic acid

: 222319-96-2
1,4-bisbutanediol

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 80 - 90 °C

2: 0.25 h / 130 - 140 °C

With thionyl chloride;
DOI:10.1021/jm9804735