1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide

Base Information

Chemical Name:1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide
CAS No.:1403575-24-5
Molecular Formula:Br*C₃₀H₄₅N₄O
Molecular Weight:557.618
Hs Code.:

Synonyms:

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Chemical Property of 1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide

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Technology Process of 1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide

There total 5 articles about 1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 616-47-7
1-methyl-1H-imidazole

: 1403575-07-4
2-[3-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

: 1403575-24-5
1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide

Guidance literature:: In acetonitrile; at 60 ℃; for 72h; Inert atmosphere;
DOI:10.1039/c2jm34595a

Reference yield:

: 14620-53-2
1,1-dimethoxytetradecane

: 1403575-24-5
1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 40 °C / Inert atmosphere; Cooling with ice

1.2: 2 h / 40 - 60 °C / Inert atmosphere

2.1: sodium methylate / methanol / 14 h / 20 °C / Inert atmosphere; Reflux

3.1: potassium hydroxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

3.2: 12 h / 20 °C / Inert atmosphere

4.1: acetonitrile / 72 h / 60 °C / Inert atmosphere

With sodium methylate; potassium hydroxide; trichlorophosphate; In methanol; dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c2jm34595a

Reference yield:

: 1403575-02-9
3-(5-dodecylpyrimidin-2-yl)phenol

: 1403575-24-5
1-{4-[3-(5-dodecylpyrimidin-2-yl)phenoxy]butyl}-3-methylimidazolium bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: acetonitrile / 72 h / 60 °C / Inert atmosphere

With potassium hydroxide; In dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c2jm34595a