1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane

Base Information

Chemical Name:1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane
CAS No.:1075738-16-7
Molecular Formula:C₁₇H₁₄F₆Ge
Molecular Weight:404.879
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane

Chemical Property:

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Technology Process of 1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane

There total 1 articles about 1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 402-51-7
4-(trifluoromethyl)phenylmagnesium bromide

: 10038-98-9
germaniumtetrachloride

: 62934-64-9
1,3-bis(bromomagnesio)propane

: 1075738-16-7
1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane

Guidance literature:: In diethyl ether; byproducts: (CF3C6H4)3GeCl, (CF3C6H4)GeCl3; treatment of germanium tetrachloride with trifluoromethylphenylmagnesiumbromide, treatment with obtained germanium compd. with dimagnesium comp d. in ether; chromy., recrystn. (methanol), NMR and MS;
DOI:10.1021/om800574s

Reference yield:

: 67-56-1
methanol

: 1075738-16-7
1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane

: 1075738-24-7
(4-trifluoromethylphenyl)2Ge(CH₃)(methoxy)

Guidance literature:: In hexane; Irradiation (UV/VIS); photolysis at 248 nm of germanium compd. in air satd. hexane in presenceof methanol at 25°C; UV monitoring; Kinetics;
DOI:10.1021/om800574s

Reference yield:

: 1075738-16-7
1,1'-bis(4-(trifluoromethyl)phenyl)germacyclobutane

: 64-19-7,77671-22-8
acetic acid

: (4-trifluoromethylphenyl)2Ge(CH₃)(OAc)

Guidance literature:: In acetonitrile; Irradiation (UV/VIS); photolysis at 248 nm of germanium compd. in CH3CN in presence of acetic acid at 25, 45 and 60°C; UV monitoring; Kinetics;
DOI:10.1021/om800574s