C₂₃H₂₄N₄O₂

Base Information

Chemical Name:C₂₃H₂₄N₄O₂
CAS No.:1349068-06-9
Molecular Formula:C₂₃H₂₄N₄O₂
Molecular Weight:388.469
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₃H₂₄N₄O₂

Chemical Property:

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Technology Process of C₂₃H₂₄N₄O₂

There total 8 articles about C₂₃H₂₄N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₄N₄O₂

: 64-19-7,77671-22-8
acetic acid

: 1349068-06-9
C₂₃H₂₄N₄O₂

Guidance literature:: C₂₁H₂₄N₄O₂; acetic acid; With 1-methyl-pyrrolidin-2-one; isobutyl chloroformate; In tetrahydrofuran; for 5h; Inert atmosphere; Cooling with ice;

In tetrahydrofuran; butan-1-ol; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201307803

Reference yield:

: 71989-14-5
Fmoc-(tBu)Asp-OH

: 1349068-06-9
C₂₃H₂₄N₄O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 24 h / 40 °C / Inert atmosphere

2.1: piperidine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

3.1: acetic acid / ethanol / 2 h / 80 °C / Inert atmosphere

4.1: Lawessons reagent / toluene / 4 h / Inert atmosphere; Reflux

5.1: hydrazine hydrate / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice

6.1: 1-methyl-pyrrolidin-2-one; isobutyl chloroformate / tetrahydrofuran / 5 h / Inert atmosphere; Cooling with ice

6.2: 12 h / 90 °C / Inert atmosphere

With piperidine; Lawessons reagent; 1-methyl-pyrrolidin-2-one; hydrazine hydrate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isobutyl chloroformate; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201307803

Reference yield:

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 1349068-06-9
C₂₃H₂₄N₄O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 24 h / 40 °C / Inert atmosphere

2.1: piperidine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

3.1: acetic acid / ethanol / 2 h / 80 °C / Inert atmosphere

4.1: Lawessons reagent / toluene / 4 h / Inert atmosphere; Reflux

5.1: hydrazine hydrate / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice

6.1: 1-methyl-pyrrolidin-2-one; isobutyl chloroformate / tetrahydrofuran / 5 h / Inert atmosphere; Cooling with ice

6.2: 12 h / 90 °C / Inert atmosphere

With piperidine; Lawessons reagent; 1-methyl-pyrrolidin-2-one; hydrazine hydrate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isobutyl chloroformate; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201307803