2-Benzoyl-1-methyl-1H-indole

Base Information

Chemical Name:2-Benzoyl-1-methyl-1H-indole
CAS No.:1025-99-6
Molecular Formula:C16H13NO
Molecular Weight:235.285
Hs Code.:2933990090
Mol file:1025-99-6.mol

Synonyms:1-Methyl-2-benzoylindole;(1-methyl-indol-2-yl)-phenyl-methanone;(1-Methyl-indol-2-yl)-phenyl-keton;2-Benzoyl-1-methyl-1H-indole;(1-methyl-indol-2-yl)-phenyl ketone;Indole,2-benzoyl-1-methyl;2-benzoyl-1-methylindole;(1-methyl-1H-indol-2-yl)(phenyl)methanone;Phenyl 1-methylindol-2-yl ketone;

Suppliers and Price of 2-Benzoyl-1-methyl-1H-indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 2-Benzoyl-1-methyl-1H-indole

Chemical Property:

PSA：22.00000
LogP:3.40930

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Benzoyl-1-methyl-1H-indole

There total 12 articles about 2-Benzoyl-1-methyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.6%

: 548489-89-0
N-methoxy-N-methyl-1-methylindole-2-carboxamide

: 591-51-5
phenyllithium

: 1025-99-6
(1-methyl-1H-indol-2-yl)(phenyl)methanone

Guidance literature:: In tetrahydrofuran; hexane; water; at -78 - 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: 603-76-9
1-methylindole

: 108-86-1,52753-63-6
bromobenzene

: 65136-45-0
2-ethyl-1-methyl-1H-indole

: 3558-24-5
1-methyl-2-phenyl-1H-indole

: 1025-99-6
(1-methyl-1H-indol-2-yl)(phenyl)methanone

Guidance literature:: With triethyl borane; tert.-butyl lithium; bis-triphenylphosphine-palladium(II) chloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, pentane, hexane, r.t., 1 h; -20 deg C, 1 h, 2.) xylene, CO, 15 atm., 90 deg C, 60 h;
DOI:10.1021/jo00088a060

Reference yield:

: 603-76-9
1-methylindole

: 591-50-4
iodobenzene

: 65136-45-0
2-ethyl-1-methyl-1H-indole

: 3558-24-5
1-methyl-2-phenyl-1H-indole

: 1025-99-6
(1-methyl-1H-indol-2-yl)(phenyl)methanone

Guidance literature:: With triethyl borane; tert.-butyl lithium; bis-triphenylphosphine-palladium(II) chloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, pentane, hexane, r.t., 1 h; -20 deg C, 1 h, 2.) THF, CO, 1 atm., reflux, 20 h;
DOI:10.1021/jo00088a060