Technology Process of C16H12ClNO2
There total 4 articles about C16H12ClNO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sode de l'acide trichloroisocyanurique; sodium hydroxide;
In
methanol; water;
for 2h;
Inert atmosphere;
DOI:10.1021/jm201179h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diphenyl ether-biphenyl eutectic / 0.5 h / 240 °C / Inert atmosphere
2: sode de l'acide trichloroisocyanurique; sodium hydroxide / methanol; water / 2 h / Inert atmosphere
With
diphenyl ether-biphenyl eutectic; sode de l'acide trichloroisocyanurique; sodium hydroxide;
In
methanol; water;
DOI:10.1021/jm201179h
- Guidance literature:
-
Multi-step reaction with 4 steps
1: niobium pentachloride / dichloromethane / 48 h / 20 °C / Inert atmosphere
2: acetic acid / ethanol / Inert atmosphere; Reflux
3: diphenyl ether-biphenyl eutectic / 0.5 h / 240 °C / Inert atmosphere
4: sode de l'acide trichloroisocyanurique; sodium hydroxide / methanol; water / 2 h / Inert atmosphere
With
diphenyl ether-biphenyl eutectic; niobium pentachloride; sode de l'acide trichloroisocyanurique; acetic acid; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water;
DOI:10.1021/jm201179h