C₈H₉⁽²⁾HO

Base Information

• Chemical Name: C₈H₉⁽²⁾HO
• CAS No.: 1246182-86-4
• Molecular Formula: C₈H₁₀O
• Molecular Weight: 123.159
• Mol file: 1246182-86-4.mol

Synonyms:

Chemical Property of C₈H₉⁽²⁾HO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₈H₉⁽²⁾HO

There total 5 articles about C₈H₉⁽²⁾HO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

d(4)-methanol (811-98-3) + C10H10Cl3NO → C8H9(2)HO + C8H9(2)HO (1246182-86-4) + C9H9(2)H3O + C9H9(2)H3O

Guidance literature:

With 6C₃₈H₄₀N₄O₈^(4-)*12K⁽¹⁺⁾*4Ga⁽³⁺⁾; water-d2; In aq. phosphate buffer; at 25 ℃; for 96h; pH=8; Overall yield = 78 %; Inert atmosphere; Schlenk technique;

DOI:10.1021/ja508799p

Reference yield:

d(4)-methanol (811-98-3) + (R)-1-chloro-1-phenylethane (1459-15-0) → C8H9(2)HO + C8H9(2)HO (1246182-86-4) + C9H9(2)H3O + C9H9(2)H3O

Guidance literature:

With water-d2; In aq. phosphate buffer; at 25 ℃; for 1h; pH=8; Overall yield = 84 %; Inert atmosphere; Schlenk technique;

DOI:10.1021/ja508799p

Reference yield:

d(4)-methanol (811-98-3) + 1-phenylethyl 2,2,2-trichloroacetimidate (99421-72-4) → C8H9(2)HO + C8H9(2)HO (1246182-86-4) + C9H9(2)H3O + C9H9(2)H3O

Guidance literature:

With K₁₂(Ga₄(1,5-bis(2,3-dihydroxybenzamido)naphthalene))6; water-d2; In aq. phosphate buffer; at 50 ℃; for 24h; pH=8; Overall yield = 94 %; Inert atmosphere; Schlenk technique;

DOI:10.1021/ja508799p

upstream raw materials:

d⁽⁴⁾-methanol

(R)-1-phenylethanol picolinic acid ester

(R)-1-chloro-1-phenylethane

(S)-1-phenylethanol

Refernces

• 1、 Kannappan,Nicholas. "Selection of chiral zinc catalysts for the kinetic resolution of esters via dynamic templating". . p. 90 - 100. Retrieved 2013/04/10.