Gemcitabine hydrochloride

Base Information

• Chemical Name: Gemcitabine hydrochloride
• CAS No.: 12211-03-9
• Molecular Formula: SiZr
• Molecular Weight: 119.309
• Mol file: 12211-03-9.mol

Synonyms:

Chemical Property of Gemcitabine hydrochloride

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Gemcitabine hydrochloride

There total 16 articles about Gemcitabine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

zirconium (7440-67-7) + silicon (7440-21-3) → ZrSi (12211-03-9) + ZrSi2

Guidance literature:

With aluminium; In melt; Inert atmosphere; Electric arc;

DOI:10.1016/j.jallcom.2016.09.142

Reference yield:

zirconium (7440-67-7) + aluminium (7429-90-5) + silicon (7440-21-3) → ZrSi (12211-03-9) + ZrSi2

Guidance literature:

In melt; Inert atmosphere; Electric arc;

DOI:10.1016/j.jallcom.2016.09.142

Reference yield:

zircon + silica gel (112926-00-8,7631-86-9) → silane-treated zirconia-silica (12211-03-9) + zirconium silicide (12039-90-6)

Guidance literature:

zircon; silica gel; at 900 ℃; for 3h; Milling; Green chemistry;

With CaCl₂-NaCl eutectic molten salt; at 800 ℃; for 15h; Electrochemical reaction; Green chemistry;

DOI:10.1039/c5nj01896j

upstream raw materials:

zirconium(IV) oxide

silicon

zirconium

silica gel

Refernces

• 1、 Liu, Ya,Tang, Maoyou,Wu, Changjun,Wang, Jianhua,Su, Xuping. "Progress on phase equilibria of the Al[sbnd]Si[sbnd]Zr system at 700 and 900 °C". . p. 357 - 365. Retrieved 2017.
• 2、 Blanchard, Peter E.R.,Cavell, Ronald G.,Mar, Arthur. "Electronic structure of ZrCuSiAs and ZrCuSiP by X-ray photoelectron and absorption spectroscopy". . p. 1536 - 1544. Retrieved 2010.
• 3、 Liu, Hongxia,Cai, Yanqing,Xu, Qian,Song, Qiushi,Liu, Huijun. "A novel preparation of Zr-Si intermetallics by electrochemical reduction of ZrSiO4 in molten salts". . p. 9969 - 9975. Retrieved 2015/12/01.