2-{3-[4-(3-Chloro-phenyl)-piperazin-1-yl]-1,1-dioxo-1H-1λ⁶-benzo[b]thiophen-2-yl}-benzenesulfinic acid; compound with 1-(3-chloro-phenyl)-piperazine

Base Information

• Chemical Name: 2-{3-[4-(3-Chloro-phenyl)-piperazin-1-yl]-1,1-dioxo-1H-1λ⁶-benzo[b]thiophen-2-yl}-benzenesulfinic acid; compound with 1-(3-chloro-phenyl)-piperazine
• CAS No.: 74671-83-3
• Molecular Formula: C₁₀H₁₃ClN₂*C₂₄H₂₁ClN₂O₄S₂
• Molecular Weight: 697.706

Synonyms:

Chemical Property of 2-{3-[4-(3-Chloro-phenyl)-piperazin-1-yl]-1,1-dioxo-1H-1λ⁶-benzo[b]thiophen-2-yl}-benzenesulfinic acid; compound with 1-(3-chloro-phenyl)-piperazine

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 2-{3-[4-(3-Chloro-phenyl)-piperazin-1-yl]-1,1-dioxo-1H-1λ⁶-benzo[b]thiophen-2-yl}-benzenesulfinic acid; compound with 1-(3-chloro-phenyl)-piperazine

There total 2 articles about 2-{3-[4-(3-Chloro-phenyl)-piperazin-1-yl]-1,1-dioxo-1H-1λ⁶-benzo[b]thiophen-2-yl}-benzenesulfinic acid; compound with 1-(3-chloro-phenyl)-piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Benzothieno<3,2-b>benzothiophene Disulfone (74102-22-0) + N-(m-chlorophenyl)piperazine (6640-24-0) → 2-{3-[4-(3-Chloro-phenyl)-piperazin-1-yl]-1,1-dioxo-1H-1λ6-benzo[b]thiophen-2-yl}-benzenesulfinic acid; compound with 1-(3-chloro-phenyl)-piperazine (74671-83-3)

Guidance literature:

In benzene; for 8h; Heating;

DOI:10.1007/BF02401716

Reference yield:

benzthieno[3,2-b]benzothiophene (248-70-4) → 2-{3-[4-(3-Chloro-phenyl)-piperazin-1-yl]-1,1-dioxo-1H-1λ6-benzo[b]thiophen-2-yl}-benzenesulfinic acid; compound with 1-(3-chloro-phenyl)-piperazine (74671-83-3)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O₂

2: 76 percent / benzene / 8 h / Heating

With dihydrogen peroxide; In benzene;

DOI:10.1007/BF02401716

upstream raw materials:

Benzothieno<3,2-b>benzothiophene Disulfone

N-(m-chlorophenyl)piperazine

benzthieno[3,2-b]benzothiophene

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