diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Base Information

Chemical Name:diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate
CAS No.:872216-21-2
Molecular Formula:C₂₇H₂₅N₃PPd*C₃₂H₁₂BF₂₄
Molecular Weight:1392.13
Hs Code.:

diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

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Chemical Property of diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

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Technology Process of diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

There total 1 articles about diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 872216-16-5
diphenylphosphino(phenyl pyridin-2-yl-methylene)amine palladium methyl chloride

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 872216-21-2
diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Guidance literature:: In acetonitrile; (N2); using Schlenk techniques; sealing of mixt. of Pd(C5H4NC(Ph)NPPh2)Cl(Me), Na(B(3,5-(CF3)2-C6H3)4) and acetonitrile; sealing, stirring for 4days at room temp.; pptn., filtration, removal of solvent under reduced pressure, dissolvingin CH2Cl2, filtration, removal of solvent, drying in vac., elem. anal.;
DOI:10.1016/j.jorganchem.2005.04.032

Reference yield:

: 872216-21-2
diphenylphosphino(phenyl pyridin-2-yl-methylene)amine methyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

: 201230-82-2
carbon monoxide

: 872216-24-5
diphenylphosphino(phenyl pyridin-2-yl-methylene)amine η1-acyl acetonitrile palladium(II) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Guidance literature:: In chloroform-d1; charging of NMR tube with (C5H4NC(Ph)NPPh2)Pd(Me)(MeCN)(B(C6H3(CF3)2)4);addn. of CDCl3; freeze/thaw degassing, filling with CO; sealing; standi ng at room temp. for 6 h with vigorous shaking; monitoring by NMR;
DOI:10.1016/j.jorganchem.2005.04.032