(C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)(CH₃)

Base Information

Chemical Name:(C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)(CH₃)
CAS No.:1198298-22-4
Molecular Formula:C₃₁H₄₁CrN₂
Molecular Weight:493.676
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)Cr((C<sub>2</sub>H<sub>5</sub>)2C<sub>6</sub>H<sub>3</sub>NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(C<sub>2</sub>H<sub>5</sub>)2)(CH<sub>3</sub>)

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Chemical Property of (C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)(CH₃)

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Technology Process of (C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)(CH₃)

There total 2 articles about (C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)(CH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 917-64-6
methyl magnesium iodide

: 1198298-26-8
[Cr(cyclopentadienyl)((2,6-diethylphenyl)NC(Me)CHC(Me)N(2,6-diethylphenyl))]

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 1198298-22-4
(C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)(CH₃)

Guidance literature:: With 1,4-dioxane; In diethyl ether; under N2; solid I2 added to soln. of Cr complex in Et2O; stirred for 2 h; soln. of MeMgI in Et2O added; stirred for 1.5 h; 1,4-dioxane (excess) added; stirred for 15 min; solvent removed in vac.; extd. with pentane; filtered through Celite; rinsed with pentane; crystd. at -30°C overnight; elem. anal.;
DOI:10.1021/om900788c

Reference yield:

: 1198298-26-8
[Cr(cyclopentadienyl)((2,6-diethylphenyl)NC(Me)CHC(Me)N(2,6-diethylphenyl))]

: 74-88-4
methyl iodide

: 1198298-22-4
(C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)(CH₃)

: 1198298-19-9
(C₅H₅)Cr((C₂H₅)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(C₂H₅)2)I

Guidance literature:: In pentane; under N2; Cr complex dissolved in pentane; soln. of MeI (10 equiv.) in t-butyl methyl ether added; mixed; not isolated; monitored by UV-vis spectra; Kinetics;
DOI:10.1021/om900788c