ethyl 4-(2,5-dimethyl-6-phenylpyridin-3-yl)benzoate

Base Information

Chemical Name:ethyl 4-(2,5-dimethyl-6-phenylpyridin-3-yl)benzoate
CAS No.:1264758-34-0
Molecular Formula:C₂₂H₂₁NO₂
Molecular Weight:331.414
Hs Code.:

Synonyms:

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Chemical Property of ethyl 4-(2,5-dimethyl-6-phenylpyridin-3-yl)benzoate

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Technology Process of ethyl 4-(2,5-dimethyl-6-phenylpyridin-3-yl)benzoate

There total 2 articles about ethyl 4-(2,5-dimethyl-6-phenylpyridin-3-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5798-75-4
Ethyl 4-bromobenzoate

: 25201-44-9
2-methyl-1-phenyl-3-butene-1-ol

: 78-94-4,25038-87-3
methyl vinyl ketone

: 1264758-34-0
ethyl 4-(2,5-dimethyl-6-phenylpyridin-3-yl)benzoate

Guidance literature:: 2-methyl-1-phenyl-3-butene-1-ol; methyl vinyl ketone; With 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride; In dichloromethane; for 48h; Inert atmosphere; Reflux;

With water; Dess-Martin periodane; In dichloromethane; at 0 ℃;

Ethyl 4-bromobenzoate;
DOI:10.1021/ol103088r

Reference yield:

: 100-52-7
benzaldehyde

: 1264758-34-0
ethyl 4-(2,5-dimethyl-6-phenylpyridin-3-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium chloride; zinc / tetrahydrofuran; water / 20 °C

2.1: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / dichloromethane / 48 h / Inert atmosphere; Reflux

2.2: 0 °C

With 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride; ammonium chloride; zinc; In tetrahydrofuran; dichloromethane; water; 2.1: Olefin cross-metathesis / 2.2: Dess-Martin oxidation;
DOI:10.1021/ol103088r