Technology Process of C40H36N10O7
There total 9 articles about C40H36N10O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere
2.1: sodium hydroxide; water / methanol
3.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 0 - 20 °C
3.2: 1 h / 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane
5.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 0.17 h / Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)
5.2: Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)
With
copper(ll) sulfate pentahydrate; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; di-isopropyl azodicarboxylate; water; sodium L-ascorbate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201206281
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium azide; 18-crown-6 ether / dimethyl sulfoxide / 12 h / 25 °C
2.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 0.17 h / Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)
2.2: Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)
With
sodium azide; copper(ll) sulfate pentahydrate; 18-crown-6 ether; sodium L-ascorbate;
In
water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1002/anie.201206281
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: thionyl chloride / -10 °C / Reflux
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere
3.1: sodium hydroxide; water / methanol
4.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 0 - 20 °C
4.2: 1 h / 0 - 20 °C
5.1: trifluoroacetic acid / dichloromethane
6.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 0.17 h / Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)
6.2: Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)
With
thionyl chloride; copper(ll) sulfate pentahydrate; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; di-isopropyl azodicarboxylate; water; sodium L-ascorbate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201206281