(1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester

Base Information

Chemical Name:(1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester
CAS No.:335332-34-8
Molecular Formula:C₃₈H₄₇N₂O₈P
Molecular Weight:690.774
Hs Code.:

(1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester

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Chemical Property of (1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester

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Technology Process of (1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester

There total 3 articles about (1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 335332-34-8
(1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₃N

1.2: PCl₅ / CHCl₃

2.1: LDA

3.1: TFA

4.1: EDC; HOBt

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid; lithium diisopropyl amide;
DOI:10.1016/S0960-894X(00)00659-4

Reference yield:

: 335332-32-6
(1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-trimethylsilanyl-ethoxycarbonyl)-pentyl ester

: 335332-34-8
(1R,2R,3S,5S)-3-(Benzyloxy-phenyl-phosphinoyloxy)-8-methyl-8-aza-bicyclo[3.2.1]octane-2-carboxylic acid 5-(2-benzyloxycarbonyl-ethylcarbamoyl)-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA

2: EDC; HOBt

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid;
DOI:10.1016/S0960-894X(00)00659-4