N-[(4-Nitrobenzoyl)oxy]benzamide

Base Information

• Chemical Name: N-[(4-Nitrobenzoyl)oxy]benzamide
• CAS No.: 1037-48-5
• Molecular Formula: C14H10N2O5
• Molecular Weight: 286.244
• DSSTox Substance ID: DTXSID70559797
• Wikidata: Q82442644
• Mol file: 1037-48-5.mol

Synonyms:N-[(4-Nitrobenzoyl)oxy]benzamide;1037-48-5;DTXSID70559797

Chemical Property of N-[(4-Nitrobenzoyl)oxy]benzamide

Chemical Property:

• XLogP3: 2.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 4
• Exact Mass: 286.05897142
• Heavy Atom Count: 21
• Complexity: 393

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)NOC(=O)C2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of N-[(4-Nitrobenzoyl)oxy]benzamide

There total 7 articles about N-[(4-Nitrobenzoyl)oxy]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

potassium benzohydroxamate (32685-16-8) + 4-nitro-benzoyl chloride (122-04-3) → O-p-nitrobenzoylbenzohydroxamic acid (1037-48-5)

Guidance literature:

In 1,4-dioxane; for 0.166667h; Heating;

DOI:10.1135/cccc19932150

Reference yield: 60.0%

Benzohydroxamic acid (495-18-1) + 4-chlorobenzonitrile (100-00-5) → O-p-nitrobenzoylbenzohydroxamic acid (1037-48-5)

Guidance literature:

In pyridine; for 8h; Ambient temperature;

Reference yield:

1-nitro-1-phenylmethane (622-42-4) → O-p-nitrobenzoylbenzohydroxamic acid (1037-48-5)

Guidance literature:

With diethyl ether; isopropylmagnesium chloride; anschliessendes Behandeln mit 4-Nitro-benzoylchlorid in THF;

upstream raw materials:

1-nitro-1-phenylmethane

Benzohydroxamic acid

4-nitro-benzoyl chloride

potassium benzohydroxamate

Downstream raw materials:

N,N-diphenylurea

N-chloro-N-(4-nitrobenzoyloxy)-benzamide