C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br

Base Information

Chemical Name:C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br
CAS No.:339320-28-4
Molecular Formula:C₂₈H₂₆BrO₅Re
Molecular Weight:708.622
Hs Code.:

C<sub>5</sub>H<sub>4</sub>Re(CO)3C<sub>2</sub>H<sub>5</sub>CCC<sub>6</sub>H<sub>4</sub>OHC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)4Br

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Suppliers and Price of C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br

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Technology Process of C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br

There total 1 articles about C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 339320-27-3
cyclopentadienyltricarbonylrhenium ethyl ketone

: 339320-26-2
4-(4-Bromobutoxy)-4'-hydroxybenzophenone

: 339320-28-4,339320-30-8
C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; TiCl4 mixed with Zn at o°C, refluxed for 2 h, cooled to room temp., mixed with Re complex and benzophenone, refluxed for 2 h, cooled to room temp.; stirred with H2O and CH2Cl2, MAS;
DOI:10.1039/b009553m

Reference yield: 64.0%

: 339320-28-4,339320-30-8
C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br

: 124-40-3
dimethyl amine

: 339320-31-9,339320-29-5
C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4N(CH₃)2

Guidance literature:: In methanol; heated with stirring in autoclave at 60°C for 1 day, cooled, concd.(vac.); chromy.(Kromasil-CH3OH), MAS;
DOI:10.1039/b009553m