[((η5-2,5-Me2-3,4-Ph2C5O)Ru(CO)2)2]

Base Information

• Chemical Name: [((η5-2,5-Me2-3,4-Ph2C5O)Ru(CO)2)2]
• CAS No.: 96482-50-7
• Molecular Formula: C₄₂H₃₂O₆Ru₂
• Molecular Weight: 834.852

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Chemical Property of [((η5-2,5-Me2-3,4-Ph2C5O)Ru(CO)2)2]

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Technology Process of [((η5-2,5-Me2-3,4-Ph2C5O)Ru(CO)2)2]

There total 1 articles about [((η5-2,5-Me2-3,4-Ph2C5O)Ru(CO)2)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

dodecacarbonyl-triangulo-triruthenium (15243-33-1) + 2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone (26307-17-5) → {(C4(C6H5)2(CH3)2CO)(CO)2Ru}2 (96482-50-7)

Guidance literature:

In n-heptane; refluxing soln. of tetraphenylcyclopentadiene and Ru3(CO)12 in dry heptane (N2, ca. 40 h), monitoring course of reaction by IR; cooling, pptn., filtering; elem. anal.;

Reference yield: 91.0%

dichloromethane (75-09-2) + (η5-2,5-Me2-3,4-Ph2C5OH)RuI(CO)2 (1174232-39-3) + [((η5-2,5-Me2-3,4-Ph2C5O)Ru(CO)2)2] (96482-50-7) → [(Ru(CO)2(η5-2,5-Me2-3,4-Ph2C5OH))(Ru(CO)2(η4-2,5-Me2-3,4-Ph2C5O))(μ-I)]*2dichloromethane

Guidance literature:

In dichloromethane; (Ar, Schlenk technique); dissolving mixt. of ruthenium compds. in CH2Cl2, stirring at room temp. for 1 h; concg., washing with hexane,, NMR, MS and X-ray anal.;

DOI:10.1021/om9003434

Reference yield:

{(C4(C6H5)2(C6H4Cl)2CO)(CO)2Ru}2 (119743-33-8) + {(C4(C6H5)2(CH3)2CO)(CO)2Ru}2 (96482-50-7) → (((C4-2,5-Ph2-3,4-(p-ClC6H4)2CO))Ru)((C4-3,4-Ph2-2,5-Me2CO)(CO)2Ru)

Guidance literature:

In benzene-d6; measuring 1H NMR spectrum of soln. as a function of time (24°C or 52 degree.C);

upstream raw materials:

dodecacarbonyl-triangulo-triruthenium

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone

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