N-[(E)-[(2E)-2-(benzoylhydrazinylidene)-1,2-diphenylethylidene]amino]benzamide

Base Information

• Chemical Name: N-[(E)-[(2E)-2-(benzoylhydrazinylidene)-1,2-diphenylethylidene]amino]benzamide
• CAS No.: 36289-76-6
• Molecular Formula: C28H22 N4 O2
• Molecular Weight: 446.4999
• NSC Number: 155482
• DSSTox Substance ID: DTXSID40423496
• Mol file: 36289-76-6.mol

Synonyms:36289-76-6;N-[(E)-[(2E)-2-(benzoylhydrazinylidene)-1,2-diphenylethylidene]amino]benzamide;NSC155482;DTXSID40423496;FCYVHTSUXHTTMQ-XDHTVYJESA-N;NSC-155482;AE-018/31861060

Chemical Property of N-[(E)-[(2E)-2-(benzoylhydrazinylidene)-1,2-diphenylethylidene]amino]benzamide

Chemical Property:

• XLogP3: 5.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 446.17427596
• Heavy Atom Count: 34
• Complexity: 661

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NNC(=O)C2=CC=CC=C2)C(=NNC(=O)C3=CC=CC=C3)C4=CC=CC=C4
• Isomeric SMILES: C1=CC=C(C=C1)/C(=N\NC(=O)C2=CC=CC=C2)/C(=N/NC(=O)C3=CC=CC=C3)/C4=CC=CC=C4

Technology Process of N-[(E)-[(2E)-2-(benzoylhydrazinylidene)-1,2-diphenylethylidene]amino]benzamide

There total 1 articles about N-[(E)-[(2E)-2-(benzoylhydrazinylidene)-1,2-diphenylethylidene]amino]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ benzil bis(benzoylhydrazone) (36289-76-6)

Guidance literature:

Benzil, Benzoylhydrazin;

DOI:10.1246/bcsj.49.2606

Reference yield: 92.0%

benzil bis(benzoylhydrazone) (36289-76-6) + dimethyltin dichloride (753-73-1) → SnMe2(PhCONNCPh)2 (1251563-87-7)

Guidance literature:

With Et₃N; In dichloromethane; byproducts: Et3N*HCl; to CH2Cl2 soln. of hydrazone deriv. with 4 drops of Et3N added SnMe2Cl2 in CH2Cl2; soln. stirred overnight; soln. evapd. to dryness; Et2O added; ppt. discarded, soln. allowed to evaporate slowly; elem. anal.;

DOI:10.1016/j.jorganchem.2010.07.002

Reference yield: 87.0%

benzil bis(benzoylhydrazone) (36289-76-6) + dibutyltin chloride (683-18-1) → SnBu2(PhCONNCPh)2 (1251563-90-2)

Guidance literature:

With Et₃N; In dichloromethane; byproducts: Et3N*HCl; to CH2Cl2 soln. of hydrazone deriv. with 4 drops of Et3N added SnBu2Cl2 in CH2Cl2; soln. stirred overnight; soln. evapd. to dryness; Et2O added; ppt. discarded, soln. allowed to evaporate slowly; elem. anal.;

DOI:10.1016/j.jorganchem.2010.07.002

Downstream raw materials:

3,5,6-triphenyl-[1,2,4]triazine

{dioxouranium(VI)(benzilbis(benzoylhydrazone))(sulphate)}

{dioxouranium(VI)(benzilbis(benzoylhydrazone))(nitrate)2}

{dioxouranium(VI)(benzilbis(benzoylhydrazone))(chloride)2}