[RuCl2(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)]

Base Information

Chemical Name:[RuCl2(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)]
CAS No.:849371-32-0
Molecular Formula:C₂₄H₃₁Cl₂N₂PRu
Molecular Weight:550.473
Hs Code.:

Synonyms:

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Chemical Property of [RuCl2(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)]

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Technology Process of [RuCl2(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)]

There total 1 articles about [RuCl2(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 3999-13-1
2-diphenylphosphino-1,1-dimethylhydrazine

: 849371-32-0
[RuCl2(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)]

Guidance literature:: In tetrahydrofuran; under N2; to a soln. of a ligand (2.05 mmol) in THF Ru-contg. compd. (1.0 mmol) was added; the mixt. was heated under reflux for 1 h and then allowed to cool to room temp.; the vol. was reduced by half; the soln. was cooled to 0°C; the ppt. was isolated by filtration and washed with cold THF and pentane; the ppt. was recrystd. from CH2Cl2-pentane and dried under vac.; elem. anal.;
DOI:10.1039/b417068g

Reference yield: 89.0%

: 14104-20-2
silver tetrafluoroborate

: 849371-32-0
[RuCl2(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)]

: 849371-36-4
[RuCl(η6-p-MeC6H4(i)Pr)(2-diphenylphosphino-1,1-dimethylhydrazine)][BF4]

Guidance literature:: In toluene; byproducts: AgCl; under N2; to a soln. of Ru-contg. compd. (o.45 mmol) in toluene, AgBF4 (0.47 mmol) was added in the dark; stirring at room temp. for 30 min; the solid was isolated by filtration in the dark; the solid was dissolved in CH2Cl2 and the soln. was filtered; the vol. was reduced and Et2O was added to ppt. a solid; elem. anal.;
DOI:10.1039/b417068g